苯甲基-N,N-二甲基二硫代氨基甲酸合成路线 （共 14 条）
反应条件
sodium hydroxide; ethanol
参考文献
Kulka
Canadian Journal of Chemistry, 1956 , vol. 34, p. 1093,1099
反应条件
1: toluene With tert.-butylhydroperoxide; N-bromosuccinmide in neat (no solvent)
T=20°C; 2 h;
2: carbon disulfide; dimethyl amine in neat (no solvent)
T=20°C; 5 h;
参考文献
Guntreddi, Tirumaleswararao; Vanjari, Rajeshwer; Singh, Krishna Nand
Tetrahedron, 2014 , vol. 70, # 25 p. 3887 - 3892
反应条件
1: benzylzinc iodide With Li-N,N-dimethyldithiocarbamat
2: bis(N,N-dimethyl thiocarbamoyl)-disulphide in tetrahydrofuran; dichloromethane
T=20°C;
参考文献
Krasovskiy, Arkady; Gavryushin, Andrey; Knochel, Paul
Synlett, 2006 , # 5 p. 792 - 794
反应条件
1: dibenzyl disulphide With lithium aluminium tetrahydride in tetrahydrofuran
T=0°C; 0.5 h;
2: N,N-dimethylthiocarbamoyl chloride in tetrahydrofuran
T=0°C; 2 h;
参考文献
Koketsu, Mamoru; Otsuka, Toshihiro; Ishihara, Hideharu
Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 3 p. 443 - 448
反应条件
triphenylphosphine; diethylazodicarboxylate in toluene
Ambient temperature;
参考文献
Rollin, P.
Tetrahedron Letters, 1986 , vol. 27, # 35 p. 4169 - 4170
反应条件
in tetrahydrofuran; dichloromethane
T=20°C;
参考文献
Krasovskiy, Arkady; Gavryushin, Andrey; Knochel, Paul
Synlett, 2006 , # 5 p. 792 - 794
反应条件
in ethanol
1 h; Heating;
参考文献
Katritzky, Alan R.; Rezende, Marcos C.; Thind, Sukhpal S.
Journal of Chemical Research, Miniprint, 1980 , # 9 p. 4031 - 4040
反应条件
in ethanol
T=60°C; Substitution;
参考文献
Ohtani, Noritaka; Murakawa, Shigeki; Watanabe, Kohji; Tsuchimoto, Daisuke; Sato, Daiki
Journal of the Chemical Society. Perkin Transactions 2, 2000 , # 9 p. 1851 - 1856
参考文献
Kulka
Canadian Journal of Chemistry, 1956 , vol. 34, p. 1093,1099
反应条件
in benzene
6 h; Further byproducts given;
参考文献
Dravid, R. N.; Chande, M. S.
Journal of the Indian Chemical Society, 1983 , vol. 60, p. 855 - 857
