3-(4-乙酰氧基苯基)丙酸合成路线 （共 7 条）
反应条件
sodium hydroxide in water T=0 - 20°C;
参考文献
Ohkata, Katsuo; Tamura, Yukiko; Shetuni, Brandon B.; Takagi, Ryukichi; Miyanaga, Wataru; Kojima, Satoshi; Paquette, Leo A.
Journal of the American Chemical Society, 2004 , vol. 126, # 51 p. 16783 - 16792
反应条件
tetrahydrofuran; platinum Hydrogenation;
参考文献
Journal of Organic Chemistry, , vol. 24, p. 736,738
反应条件
1: 100 percent / K2CO3 / dimethylformamide / 23 h / 20 °C 2: 95.5 percent / LiBH4 / tetrahydrofuran / 22 h / 70 °C View Scheme
参考文献
Ohkata, Katsuo; Tamura, Yukiko; Shetuni, Brandon B.; Takagi, Ryukichi; Miyanaga, Wataru; Kojima, Satoshi; Paquette, Leo A.
Journal of the American Chemical Society, 2004 , vol. 126, # 51 p. 16783 - 16792
参考文献
Parker, Gregory D.; Seden, Peter T.; Willis, Christine L.
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3686 - 3689
反应条件
1: oxalyl chloride / CH2Cl2 / 2 h / 20 °C
2: 600 mg / pyridine / CH2Cl2 / 4 h / -20 °C
3: 55 percent / K2CO3 / methanol; H2O / 3 h / 20 °C
View Scheme
参考文献
Yang, Dan; Wong, Man-Kin; Yan, Zheng
Journal of Organic Chemistry, 2000 , vol. 65, # 13 p. 4179 - 4184
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20°C; 23 h;
参考文献
Ohkata, Katsuo; Tamura, Yukiko; Shetuni, Brandon B.; Takagi, Ryukichi; Miyanaga, Wataru; Kojima, Satoshi; Paquette, Leo A.
Journal of the American Chemical Society, 2004 , vol. 126, # 51 p. 16783 - 16792
反应条件
1: SOCl2 / CH2Cl2 / 18 h / 20 °C
2: diethyl ether; benzene / -20 - 20 °C
View Scheme
参考文献
Ohkata, Katsuo; Tamura, Yukiko; Shetuni, Brandon B.; Takagi, Ryukichi; Miyanaga, Wataru; Kojima, Satoshi; Paquette, Leo A.
Journal of the American Chemical Society, 2004 , vol. 126, # 51 p. 16783 - 16792
