4-硝基苯基二甲氨基甲酸盐合成路线 （共 11 条）
反应条件
1: 3-dimethylamino-phenol With potassium hydroxide in toluene T=90°C; 1 h; Reflux; 2: p-nitrophenyl dimethylcarbamate in toluene 3 h; Reflux; Product distribution / selectivity;
参考文献
NEON LABORATORIES LTD.; DALVI, Mahesh Bhagoji; KENNY, Rajesh Shashikant; TARADE, Pradeep Kisan; CHINCHKAR, Dattatray Krishna
Patent: WO2012/131699 A1, 2012 ;
Location in patent: Page/Page column 14 ;
反应条件
potassium carbonate in acetonitrile
5 h; Inert atmosphereReflux;
参考文献
John, Alex; Nicholas, Kenneth M.
Journal of Organic Chemistry, 2012 , vol. 77, # 13 p. 5600 - 5605
反应条件
in water; toluene
T=0 - 20°C; 3 h; Product distribution / selectivity;
参考文献
NEON LABORATORIES LTD.; DALVI, Mahesh Bhagoji; KENNY, Rajesh Shashikant; TARADE, Pradeep Kisan; CHINCHKAR, Dattatray Krishna
Patent: WO2012/131699 A1, 2012 ;
Location in patent: Page/Page column 11 ;
反应条件
potassium chloride; hydroxide in water
T=25°C; pH=11.5 - 12.8; Kinetics;
参考文献
Simanenko; Popov; Prokop'eva; Karpichev; Savelova; Suprun; Bunton
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 9 p. 1286 - 1298
反应条件
H2NO(1-); potassium chloride in water
T=25°C; pH=10.5 - 12.7; Kinetics;
参考文献
Simanenko; Popov; Prokop'eva; Karpichev; Savelova; Suprun; Bunton
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 9 p. 1286 - 1298
反应条件
potassium chloride; hydroxide in water
T=25°C; pH=11.5 - 12.8; Kinetics;
参考文献
Simanenko; Popov; Prokop'eva; Karpichev; Savelova; Suprun; Bunton
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 9 p. 1286 - 1298
反应条件
potassium chloride; hydroperoxide anion in water
T=25°C; pH=10.5 - 12.8; Kinetics;
参考文献
Simanenko; Popov; Prokop'eva; Karpichev; Savelova; Suprun; Bunton
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 9 p. 1286 - 1298
反应条件
potassium chloride in water
T=25°C; pH=10.8 - 12.8; Kinetics;
参考文献
Simanenko; Popov; Prokop'eva; Karpichev; Savelova; Suprun; Bunton
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 9 p. 1286 - 1298
反应条件
potassium chloride in water
T=25°C; pH=8.40 - 10.95; Kinetics;
参考文献
Simanenko; Popov; Prokop'eva; Karpichev; Savelova; Suprun; Bunton
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 9 p. 1286 - 1298
反应条件
potassium chloride in water
T=25°C; pH=11.70 - 13.30; Kinetics;
参考文献
Simanenko; Popov; Prokop'eva; Karpichev; Savelova; Suprun; Bunton
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 9 p. 1286 - 1298
