N-[2-(二甲氨基)-2-氧乙基]-氨基甲酸-1,1-二甲基乙酯合成路线 (共 7 条)
反应条件
zirconium tetrachloride in toluene T=120°C; 24 h; Inert atmosphereMolecular sieve;
参考文献
Tinnis, Fredrik; Lundberg, Helena; Adolfsson, Hans
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 13 p. 2531 - 2536
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine in dichloromethane
参考文献
Journal of the American Chemical Society, , vol. 129, # 43 p. 12956 - 12957
反应条件
tert.-butylhydroperoxide; Cu(ClO4)2*6H2O T=100°C; 6 h;
参考文献
Kumar, P. Santhosh; Kumar, G. Sathish; Kumar, R. Arun; Reddy, N. Veera; Rajender Reddy
European Journal of Organic Chemistry, 2013 , # 7 p. 1218 - 1222
反应条件
1: Et3N / -15 °C 2: H2O View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 17 p. 3039 - 3042
参考文献
Tetrahedron Letters, , vol. 38, # 17 p. 3039 - 3042
反应条件
1,1'-carbonyldiimidazole 1.) acetonitrile, 2.) 10 min; Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 3 p. 387 - 392
反应条件
hydrogenchloride in 1,4-dioxane
参考文献
Metrano, Anthony J.; Miller, Scott J.
Journal of Organic Chemistry, 2014 , vol. 79, # 4 p. 1542 - 1554