2'-脱氧-5-(羟甲基)胞啶合成路线 （共 17 条）
反应条件
in aq. buffer T=60°C; pH=7.4; Kinetics; Temperature;
参考文献
Schiesser, Stefan; Pfaffeneder, Toni; Sadeghian, Keyarash; Hackner, Benjamin; Steigenberger, Barbara; Schroeder, Arne S.; Steinbacher, Jessica; Kashiwazaki, Gengo; Hoefner, Georg; Wanner, Klaus T.; Ochsenfeld, Christian; Carell, Thomas
Journal of the American Chemical Society, 2013 , vol. 135, # 39 p. 14593 - 14599
反应条件
in aq. buffer T=80°C; pH=7.4; Kinetics; TemperaturepH-value;
参考文献
Schiesser, Stefan; Pfaffeneder, Toni; Sadeghian, Keyarash; Hackner, Benjamin; Steigenberger, Barbara; Schroeder, Arne S.; Steinbacher, Jessica; Kashiwazaki, Gengo; Hoefner, Georg; Wanner, Klaus T.; Ochsenfeld, Christian; Carell, Thomas
Journal of the American Chemical Society, 2013 , vol. 135, # 39 p. 14593 - 14599
反应条件
1: aq. buffer / 80 °C / pH 7.4 2: aq. buffer / 60 °C / pH 7.4 View Scheme
参考文献
Schiesser, Stefan; Pfaffeneder, Toni; Sadeghian, Keyarash; Hackner, Benjamin; Steigenberger, Barbara; Schroeder, Arne S.; Steinbacher, Jessica; Kashiwazaki, Gengo; Hoefner, Georg; Wanner, Klaus T.; Ochsenfeld, Christian; Carell, Thomas
Journal of the American Chemical Society, 2013 , vol. 135, # 39 p. 14593 - 14599
反应条件
sodium tetrahydroborate in methanol
Ambient temperature;
参考文献
Bienvenu, Carine; Wagner, J. Richard; Cadet, Jean
Journal of the American Chemical Society, 1996 , vol. 118, # 46 p. 11406 - 11411
反应条件
cytosine nucleoside phosphorylase in water
T=50°C; pH=8.0; 1 h; Aqueous acetate bufferEnzymatic reaction;
参考文献
Mitsui Chemicals, Inc.
Patent: US2005/74857 A1, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
1: With sodium periodate in water-d2
0.166667 h; aq. phosphate buffer;
2: in water-d2
T=37°C; 4 h;
参考文献
Peng, Xiaohua; In, Seok Hong; Li, Hong; Seidman, Michael M.; Greenberg, Marc M.
Journal of the American Chemical Society, 2008 , vol. 130, # 31 p. 10299 - 10306
反应条件
1: 13 percent / air, 2-methyl-1,4-naphthoquinone / H2O / 1 h / Ambient temperature; Irradiation
2: 74 percent / NaBH4 / methanol / Ambient temperature
View Scheme
参考文献
Bienvenu, Carine; Wagner, J. Richard; Cadet, Jean
Journal of the American Chemical Society, 1996 , vol. 118, # 46 p. 11406 - 11411
反应条件
triethylamine hydrofluoric acid in dichloromethane
T=0 - 20°C;
参考文献
Muenzel, Martin; Globisch, Daniel; Brueckl, Tobias; Wagner, Mirko; Welzmiller, Veronika; Michalakis, Stylianos; Mueller, Markus; Biel, Martin; Carell, Thomas
Angewandte Chemie - International Edition, 2010 , vol. 49, # 31 p. 5375 - 5377
反应条件
sodium peroxodisulphate in water
T=75°C; 4 h; sodium phosphate buffer pH 7.0;
参考文献
Itahara, Toshio
Chemistry Letters, 1991 , p. 1591 - 1594
反应条件
sodium peroxodisulphate
参考文献
Benner, Steven Albert
Patent: US7563887 B1, 2009 ;
Location in patent: Page/Page column 7 ;
