4-叔丁基二高氧杯[4]芳烃合成路线 (共 8 条)
反应条件
potassium hydroxide in xylene
4 h; Heating;
参考文献
Gutsche,C.D.; Dhawan,B.; No,K.H.
Journal of the American Chemical Society, 1981 , vol. 103, p. 3782
反应条件
sodium hydroxide in xylene
4 h; Heating; Yields of byproduct given;
参考文献
Gutsche,C.D.; Dhawan,B.; No,K.H.
Journal of the American Chemical Society, 1981 , vol. 103, p. 3782
反应条件
in xylene
4 h; Heating;
参考文献
Dhawan, Balram; Gutsche, C. David
Journal of Organic Chemistry, 1983 , vol. 48, # 9 p. 1536 - 1539
反应条件
1: 48.5 percent / 25percent NaOH / dioxane; methanol / 48 h / 50 - 60 °C
2: 96 percent / xylene / 4 h / Heating
View Scheme
参考文献
Dhawan, Balram; Gutsche, C. David
Journal of Organic Chemistry, 1983 , vol. 48, # 9 p. 1536 - 1539
反应条件
potassium hydroxide in xylene
4 h; Heating; Yield given. Yields of byproduct given;
参考文献
Dhawan, Balram; Gutsche, C. David
Journal of Organic Chemistry, 1983 , vol. 48, # 9 p. 1536 - 1539
反应条件
potassium hydroxide in xylene
4 h; Heatingfurther bases (NaOH, CsOH, Mg(OH)2, Ca(OH)2, Ba(OH)2, LiOH, K2CO3); further solvents, effect of the heating rate; further substituted phenols; Product distributionMechanism;
参考文献
Gutsche,C.D.; Dhawan,B.; No,K.H.
Journal of the American Chemical Society, 1981 , vol. 103, p. 3782
反应条件
potassium hydroxide in xylene
4 h; Heatingfurther bases (NaOH, CsOH, Mg(OH)2, Ca(OH)2, Ba(OH)2, LiOH, K2CO3); further solvents, effect of the heating rate; further substituted phenols; Product distributionMechanism;
参考文献
Gutsche,C.D.; Dhawan,B.; No,K.H.
Journal of the American Chemical Society, 1981 , vol. 103, p. 3782
反应条件
in xylene
T=120°C; 8 h; Product distribution; Further Variations:reaction times;
参考文献
Masci
Journal of Organic Chemistry, 2001 , vol. 66, # 4 p. 1497 - 1499