4,4'-二氨基二苯二硫醚合成路线 （共 62 条）
反应条件
ethanol; ethylene glycol; disodium disulfide
参考文献
Journal of Organic Chemistry, , vol. 13, p. 690,691, 693
反应条件
1: 2-methyl-propan-2-ol; H2O / 1.5 h / 20 - 25 °C / Irradiation; DRL-400 mercury lamp (400 W) 2: KOH / H2O / 0.33 h / Heating 3: air / H2O / 3 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 17, p. 1926 - 1935
Zhurnal Organicheskoi Khimii, , vol. 17, # 10 p. 2161 - 2170
反应条件
disulfur dichloride T=100°C; entstehen 4.4'-Bis-acetamino-diphenyldisulfid (a) und 4.4'-Bis-acetamino-diphenyltrisulfid (b);aus der Loesung des Produktes in Eisessig krystallisiert das (b);das (a) zerlegt man durch Erhitzen mit verd.Schwefelsaeure;
参考文献
Chemische Berichte, , vol. 11, p. 1173
反应条件
air in water 3 h; Ambient temperature; Yield given;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 17, p. 1926 - 1935
Zhurnal Organicheskoi Khimii, , vol. 17, # 10 p. 2161 - 2170
反应条件
1: 2-methyl-propan-2-ol; H2O / 2 h / 20 - 25 °C / Irradiation; DRL-400 mercury lamp (400 W) 2: KOH / H2O / 0.33 h / Heating 3: air / H2O / 3 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 17, p. 1926 - 1935
Zhurnal Organicheskoi Khimii, , vol. 17, # 10 p. 2161 - 2170
反应条件
1: 2-methyl-propan-2-ol; H2O / 3 h / 20 - 25 °C / Irradiation; DRL-400 mercury lamp (400 W) 2: KOH / H2O / 0.33 h / Heating 3: air / H2O / 3 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 17, p. 1926 - 1935
Zhurnal Organicheskoi Khimii, , vol. 17, # 10 p. 2161 - 2170
反应条件
sulfur T=170 - 180°C;
参考文献
Chemische Berichte, , vol. 38, p. 1131,1134
Chemische Berichte, , vol. 39, p. 2429
反应条件
hydrogenchloride; ethanol
参考文献
Journal of the Chemical Society, , p. 826,828
反应条件
triphenylphosphine in toluene T=68.4 - 87.7°C; Kinetics;
参考文献
Z. Naturforsch., B: Anorg. Chem., Org. Chem., Biochem., Biophys.,, , vol. 23, p. 1030 - 1033
反应条件
1: sulfuric acid mono-<2-amino-ethyl ester>; aqueous KOH-solution / 140 °C 2: aqueous hydrochloric acid; ethanol View Scheme
参考文献
Journal of the Chemical Society, , p. 826,828
