4,4'-二氨基二苯二硫醚合成路线 （共 62 条）
反应条件
1: With potassium 5-methyl-1,3,4-oxadiazole-2-thiolate in N,N-dimethyl-formamide T=20°C; 0.333333 h; 2: With copper(l) chloride in N,N-dimethyl-formamide T=130°C; 7 h;
参考文献
Soleiman-Beigi, Mohammad; Mohammadi, Fariba
Tetrahedron Letters, 2012 , vol. 53, # 52 p. 7028 - 7030
反应条件
iodine in methanol; water T=20°C;
参考文献
WO2013/45280 A1, ;
Page/Page column 101 ;
反应条件
ammonium hydroxide in 1,4-dioxane T=100°C; sealed ampoule;
参考文献
Rybin, A. G.; Zil'berman, E. N.; Zhivoderov, A. V.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 8 p. 1863 - 1867,1677 - 1680
反应条件
p-methoxybenzenetellurinic acid anhydride in dichloromethane 0.16 h; Ambient temperature;
参考文献
Hajipoura; Bagheri, Hamid; Ruoho, Arnold E.
Journal of Chemical Research, 2004 , # 4 p. 286 - 287
反应条件
sodium sulfide; water
参考文献
US1933217 , ;
FR714682 , ;
反应条件
tetrabutyl ammonium fluoride; palladium diacetate; NAF in water T=150°C; 0.333333 h; Microwave irradiation;
参考文献
Synlett, , # 18 p. 2733 - 2736
反应条件
hydrogen sulfide; tetraethylammonium hydroxide in methanol T=20°C; P=750.06 Torr; 0.166667 h; other halonitrobenzenes and tetraalkylammonium hydroxide, var. pressure and time; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 40, # 9.2 p. 1901 - 1903
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 9 p. 2143 - 2145
反应条件
ethanol; nickel Hydrogenation;
参考文献
Doklady Akademii Nauk SSSR, , vol. 65, p. 857,859
Chem. Zentralbl., , vol. 120, p. 6179
反应条件
1: 4-aminophenylmercaptan With n-butyllithium in tetrahydrofuran 2: (4-chlorophenyl)sulfenyl chloride in tetrahydrofuran
参考文献
Journal of the American Chemical Society, , vol. 129, # 7 p. 1888 - 1889
反应条件
hydrogenchloride; sulfur T=150°C; laesst weitere 6-Stdn.gelinde Kochen;
参考文献
Chemische Berichte, , vol. 39, p. 2429
Chemische Berichte, , vol. 27, p. 2814
Chemische Berichte, , vol. 38, p. 1433
