alpha-乙烯基苄基乙酸酯合成路线 （共 52 条）
反应条件
1.1: (SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium / dichloromethane / 80 °C / Inert atmosphere; Microwave irradiation 1.2: 2 h / 20 °C / Inert atmosphere; Microwave irradiation 2.1: iron(III) chloride hexahydrate / dichloromethane; water / 4.5 h / 20 °C / Inert atmosphere 3.1: ozone / dichloromethane / -78 °C 3.2: -78 - 20 °C / Inert atmosphere 3.3: 20 °C / Inert atmosphere 4.1: tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 13, # 22 p. 6018 - 6021
反应条件
1: tetrakis(triphenylphosphine) palladium(0); trimethylsilylazide / 1,2-dichloro-ethane / 1 h / Inert atmosphere; Reflux 2: sulfur; 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,2-dichloro-ethane / 1 h / Inert atmosphere; Reflux View Scheme
参考文献
Zhou, Wang; Xu, Jiaojiao; Zhang, Liangren; Jiao, Ning
Synlett, 2011 , # 7 p. 887 - 890
反应条件
tetraethylammonium p-toluenesulfonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile Electrochemical reaction, Pb cathode, Pt anode;
参考文献
Torii, Sigeru; Tanaka, Hideo; Katoh, Tetsuo; Morisaki, Kazuo
Tetrahedron Letters, 1984 , vol. 25, # 30 p. 3207 - 3208
反应条件
samarium diiodide; isopropyl alcohol; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 1 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tabuchi, Takanori; Inanaga, Junji; Yamaguchi, Masaru
Tetrahedron Letters, 1986 , vol. 27, # 5 p. 601 - 602
反应条件
tri-ruthenium(0)dodecacarbonyl; 2-(diphenylphosphino)benzoic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene in 1,4-dioxane T=100°C; 12 h;
参考文献
Tetrahedron Letters, , vol. 49, # 33 p. 4873 - 4875
反应条件
samarium diiodide; isopropyl alcohol; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 1 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tabuchi, Takanori; Inanaga, Junji; Yamaguchi, Masaru
Tetrahedron Letters, 1986 , vol. 27, # 5 p. 601 - 602
反应条件
acetyl chloride in ethanol T=23°C; 0.166667 h;
参考文献
Yadav, Veejendra K.; Ganesh Babu
Tetrahedron, 2003 , vol. 59, # 46 p. 9111 - 9116
参考文献
Kishali, Nurhan; Polat, M. Fatih; Altundas, Ramazan; Kara, Yunus
Helvetica Chimica Acta, 2008 , vol. 91, # 1 p. 67 - 72
反应条件
1: With ozone in dichloromethane T=-78°C; 2: With triphenylphosphine in dichloromethane 3: With triethylamine in dichloromethane T=-78 - 20°C; 8 h;
参考文献
Hon, Yung-Son; Wong, Ying-Chieh; Wu, Kuo-Jui
Journal of the Chinese Chemical Society, 2008 , vol. 55, # 4 p. 896 - 914
反应条件
tri-ruthenium(0)dodecacarbonyl; 2-(diphenylphosphino)benzoic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene in 1,4-dioxane T=100°C; 12 h;
参考文献
Kawatsura, Motoi; Ata, Fumio; Hirakawa, Takuya; Hayase, Shuichi; Itoh, Toshiyuki
Tetrahedron Letters, 2008 , vol. 49, # 33 p. 4873 - 4875
