2,3,4,5-四氢-1H-2-苯并氮杂卓合成路线 （共 18 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 24 h; Heating;
参考文献
Meyers, A. I.; Hutchings, Richard H.
Tetrahedron, 1993 , vol. 49, # 9 p. 1807 - 1820
反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride in benzene T=80°C; 10 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1977 - 1982
反应条件
1: sodium azide; hydrogenchloride / 24 h / 0 - 20 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 20 - 70 °C / |Cooling with ice View Scheme
参考文献
ACS Medicinal Chemistry Letters, , vol. 3, # 11 p. 914 - 919
反应条件
1: NH4OH 2: NaBH4, HOAc 3: 30 percent / PPh3, Pd(OAc)2 4: 81 percent / lithium aluminium hydride / tetrahydrofuran / 24 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 49, # 9 p. 1807 - 1820
反应条件
1: SOCl2 2: NH4OH 3: NaBH4, HOAc 4: 30 percent / PPh3, Pd(OAc)2 5: 81 percent / lithium aluminium hydride / tetrahydrofuran / 24 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 49, # 9 p. 1807 - 1820
反应条件
1: NaBH4, HOAc 2: 30 percent / PPh3, Pd(OAc)2 3: 81 percent / lithium aluminium hydride / tetrahydrofuran / 24 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 49, # 9 p. 1807 - 1820
反应条件
1: 30 percent / PPh3, Pd(OAc)2 2: 81 percent / lithium aluminium hydride / tetrahydrofuran / 24 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 49, # 9 p. 1807 - 1820
反应条件
1: BH3 2: 30 percent / PPh3, Pd(OAc)2 3: 81 percent / lithium aluminium hydride / tetrahydrofuran / 24 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 49, # 9 p. 1807 - 1820
反应条件
2: BH3 3: 30 percent / PPh3, Pd(OAc)2 4: 81 percent / lithium aluminium hydride / tetrahydrofuran / 24 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 49, # 9 p. 1807 - 1820
反应条件
hydrogenchloride; lithium aluminium tetrahydride; sodium azide 2.) THF, reflux, 12 h; Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Medicinal Chemistry, , vol. 39, # 18 p. 3539 - 3546
