N-Boc-L-苯丙氨醛合成路线 （共 60 条）
反应条件
diisobutylaluminium hydride in toluene T=-78°C; 2 h;
参考文献
Synthetic Communications, , vol. 22, # 7 p. 979 - 985
反应条件
Dess-Martin periodane in dichloromethane T=20°C; 2.67 h;
参考文献
US2009/42867 A1, ;
Page/Page column 33 ;
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=-78°C; Reduction;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 10, # 20 p. 2305 - 2309
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; 2 h;
参考文献
Organic letters, , vol. 3, # 6 p. 897 - 899
反应条件
hydrogen; palladium on activated charcoal in ethylene glycol dimethyl ether; ethanol T=20°C; Reduction; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 64, # 24 p. 8962 - 8964
反应条件
2,6-dimethylpyridine; triethylsilane; palladium on activated charcoal in acetone T=20°C;
参考文献
Synthesis, , # 8 p. 1121 - 1123
反应条件
1: NaHCO3 / sonification 2: DIBAL-H / CH2Cl2 / -78 °C View Scheme
参考文献
Synlett, , # 3 p. 435 - 439
反应条件
pyridine; sulfur trioxide; dimethyl sulfoxide
参考文献
Journal of the American Chemical Society, , vol. 111, # 14 p. 5463 - 5465
反应条件
1: CH2Cl2 2: (COCl)2; DMSO; iPr2NEt / CH2Cl2 / -35 - 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 22 p. 7609 - 7611
反应条件
diisobutylaluminium hydride in hexane; dichloromethane T=-78°C; 0.1 h;
参考文献
European Journal of Medicinal Chemistry, , vol. 30, # 10 p. 789 - 800
