2-溴-3,5,6-三甲基-2,5-环己二烯-1,4-二酮合成路线 （共 7 条）
反应条件
N,N,N-trimethyl-1-phenylmethanaminium tribromide in water; acetic acid
T=40°C; 5 h;
参考文献
Kajigaeshi, Shoji; Morikawa, Yukihiro; Fujisaki, Shizuo; Kakinami, Takaaki; Nishihira, Keigo
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 1 p. 336 - 338
反应条件
ammonium cerium(IV) nitrate in solid
2 h; ultrasonic irradiation;
参考文献
Morey; Saa
Tetrahedron, 1993 , vol. 49, # 1 p. 105 - 112
反应条件
tetrachloromethane; bromine
参考文献
Smith; Miller
Journal of the American Chemical Society, 1942 , vol. 64, p. 440,442
反应条件
hydrogenchloride; acetic acid; tin(ll) chloride
Erhitzen des erhaltenen 6-Brom-2.3.5-trimethyl-p-phenylendiamin-chlorostannats mit FeCl3 in wss. HCl;
参考文献
Smith; Johnson
Journal of the American Chemical Society, 1937 , vol. 59, p. 673,678
反应条件
1: concentrated H2SO4; chloroform; HNO3 / -5 - 0 °C
2: acetic acid; SnCl2; aqueous HCl / Erhitzen des erhaltenen 6-Brom-2.3.5-trimethyl-p-phenylendiamin-chlorostannats mit FeCl3 in wss. HCl
View Scheme
参考文献
Smith; Johnson
Journal of the American Chemical Society, 1937 , vol. 59, p. 673,678
反应条件
N-bromosuccinmide in ethanol; chloroform
参考文献
Clark,V.M. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 79 - 84
反应条件
1: NBS / methanol
2: NBS / ethanol; CHCl3
View Scheme
参考文献
Clark,V.M. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 79 - 84
