N-叔丁氧羰基-L-谷氨酸 1-甲酯合成路线 （共 12 条）
反应条件
palladium dihydroxide; hydrogen in ethanol
参考文献
Tetrahedron Letters, , vol. 39, # 15 p. 2099 - 2102
反应条件
1: potassium carbonate / dimethylformamide 2: 42 g / H2 / Pd/C / ethanol View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 5, # 12 p. 1915 - 1923
反应条件
ruthenium(IV) oxide; sodium periodate in tert-butyl alcohol T=20°C; 48 h;
参考文献
Tetrahedron Letters, , vol. 49, # 17 p. 2786 - 2788
反应条件
1: 2.1 g / CH2Cl2 / 16 h 2: 98 percent / H2 / Pd/C / methanol / 12 h / 2068.59 Torr View Scheme
参考文献
Chemical Communications, , # 37 p. 4652 - 4654
反应条件
1.1: H2SO4 1.2: pyridine / ethanol 2.1: triethylamine / dimethylformamide 3.1: potassium carbonate / dimethylformamide 4.1: 42 g / H2 / Pd/C / ethanol View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 5, # 12 p. 1915 - 1923
反应条件
1: triethylamine / dimethylformamide 2: potassium carbonate / dimethylformamide 3: 42 g / H2 / Pd/C / ethanol View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 5, # 12 p. 1915 - 1923
反应条件
papain pH=4.2; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 55, # 14 p. 2274 - 2276
反应条件
(i) aq. HBr, AcOH, (ii) /BRN= 1363586/, Et3N, dioxane; Multistep reaction;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 19, p. 1708 - 1713
反应条件
1: 92 percent / N-ethylmorpholine, propylphosphonic acid anhydride 2: 100 percent / DMAP 3: 62 percent / DIBAH View Scheme
参考文献
Burkhart, Fred; Hoffmann, Matthias; Kessler, Horst
Angewandte Chemie (International Edition in English), 1997 , vol. 36, # 11 p. 1191 - 1192
反应条件
1.1: EtOCOCl; Et3N / tetrahydrofuran 1.2: NaBH4 / tetrahydrofuran; H2O 2.1: (COCl)2; DMSO; Et3N / CH2Cl2 / -78 °C 3.1: 15 percent / 1,4-diazabicyclo[2.2.2]octane / Pd(OAc)2 / dimethylformamide / 85 °C View Scheme
参考文献
Jia, Yanxing; Zhu, Jieping
Synlett, 2005 , # 16 art. no. G22605ST, p. 2469 - 2472
