硫代磷酸O,O-二甲基S-(苯基甲基)酯合成路线 （共 8 条）
反应条件
1: phenylmethanethiol With N-chloro-succinimide in acetonitrile
T=20°C; 0.333333 h; Inert atmosphere;
2: phosphonic acid dimethyl ester in acetonitrile
T=20°C; 0.166667 h; Inert atmosphere;
参考文献
Liu, Yi-Chen; Lee, Chin-Fa
Green Chemistry, 2014 , vol. 16, # 1 p. 357 - 364
反应条件
2,6-dimethylpyridine; TeCl4 in dichloromethane
3 h; -42 deg C, 5-10 min; room temp. 1 h;
参考文献
Watanabe; Inoue; Yamamoto; Ozaki
Synthesis, 1995 , # 10 p. 1243 - 1244
反应条件
in toluene
Ambient temperature;
参考文献
Muller; Roth
Tetrahedron Letters, 1990 , vol. 31, # 4 p. 501 - 502
反应条件
in toluene
Ambient temperature;
参考文献
Muller; Roth
Tetrahedron Letters, 1990 , vol. 31, # 4 p. 501 - 502
反应条件
1: SCl2 / diethyl ether
2: tetrahydrofuran / 30 h / Heating
View Scheme
参考文献
Harpp,D.N.; Smith,R.A.
Journal of Organic Chemistry, 1979 , vol. 44, p. 4140 - 4144
反应条件
N(Et)4ClO4; sodium bromide in acetonitrile
参考文献
Torii,S. et al.
Journal of Organic Chemistry, 1979 , vol. 44, p. 2938 - 2941
反应条件
in tetrahydrofuran
30 h; Heating;
参考文献
Harpp,D.N.; Smith,R.A.
Journal of Organic Chemistry, 1979 , vol. 44, p. 4140 - 4144
参考文献
Farbenfabr. Bayer
Patent: DE947367 , 1954 ;
