2-(三甲基硅甲基)烯丙基乙酸酯合成路线 (共 6 条)
反应条件
pyridine in dichloromethane T=0°C; 0.666667 h;
参考文献
Trost,B.M.; Renaut,P.
Journal of the American Chemical Society, 1982 , vol. 104, p. 6668
反应条件
1: 1N H2SO4 / tetrahydrofuran / Ambient temperature 2: 66 percent / pyridine / Ambient temperature View Scheme
参考文献
Heterocycles, , vol. 23, # 1 p. 51 - 56
反应条件
in N,N-dimethyl-formamide T=55 - 60°C; 48 h;
参考文献
Trost, Barry M.; Buch, Michael; Miller, Maria L.
Journal of Organic Chemistry, 1988 , vol. 53, # 20 p. 4887 - 4888
反应条件
1.) benzene, ether, 0 deg C, 1 h, 2.) 0 deg C to room temp., 1 h; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 24, # 9 p. 1215 - 1221
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene T=60°C; P=760.051 Torr; 20 h;
参考文献
Greco, George E.; Gleason, Brittany L.; Lowery, Tiffany A.; Kier, Matthew J.; Hollander, Lisa B.; Gibbs, Shoshanah A.; Worthy, Amanda D.
Organic Letters, 2007 , vol. 9, # 19 p. 3817 - 3820
反应条件
palladium diacetate; triphenylphosphine; Bu3SnOAc
Cycloaddition;
参考文献
Trost, Barry M.; Toste, F. Dean
Tetrahedron Letters, 1999 , vol. 40, # 44 p. 7739 - 7743