(E)-2-丁烯基乙酸酯合成路线 (共 41 条)
反应条件
formic acid; [Ru(η4-C8H12)(η6-C8H10)]; triethylamine in 1,4-dioxane T=80°C; 4 h; other allylic carboxylates and carbonates; ruthenium-catalysed reductive cleavage of allylic esters; var. conditions; Product distribution;
参考文献
Maruyama, Yooichiroh; Sezaki, Takao; Tekawa, Masafumi; Sakamoto, Toshiaki; Shimizu, Isao; Yamamoto, Akio
Journal of Organometallic Chemistry, 1994 , vol. 473, # 1-2 p. 257 - 264
反应条件
copper; Cu(II) perchlorate in tetrahydrofuran 6 h; Heating; Yield given;
参考文献
Baruah, Jubaraj B.; Samuelson, Ashoka G.
Journal of Organometallic Chemistry, 1989 , vol. 361, p. C57 - C60
反应条件
1: (E)-crotyl acetate With indium(III) chloride; dimethyl(n-butyl)amine; lithium chloride; indium; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=35°C; 2: monoiodonaphthalene in N,N-dimethyl-formamide T=100°C; Title compound not separated from byproducts;
参考文献
Lee, Phil Ho; Seomoon, Dong; Lee, Kooyeon; Kim, Sundae; Kim, Hyunseok; Kim, Hyun; Shim, Eunkyong; Lee, Miae; Lee, Seokju; Kim, Misook; Sridhar, Madabhushi
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1641 - 1645
参考文献
Talekar, D. G.; Joshi, P. L.; Ramaiah, P.; Rao, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 145 - 151
反应条件
silver hexafluoroantimonate; [{(η5-C5Me5)RhCl}2(μ-Cl)2]; copper (II) acetate monohydrate in 1,1-dimethylpropan-1-ol T=120°C; 24 h; Inert atmosphere; Reagent/catalystSolventTemperature;
参考文献
Organic Letters, , vol. 15, # 17 p. 4576 - 4579
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
Ambient temperature2-3 h;
参考文献
Fleming, Ian; Higgins, Dick; Lawrence, Nicholas J.; Thomas, Andrew P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3331 - 3350
反应条件
4 A molecular sieve; Bu4N[Fe(CO)3(NO)] in hexane
T=80°C; 5 h;
参考文献
Magens, Silja; Ertelt, Melanie; Jatsch, Anja; Plietker, Bernd
Organic Letters, 2008 , vol. 10, # 1 p. 53 - 56
反应条件
2,6-di-tert-butyl-4-methyl-phenol; ethanesulfonic acid in water
T=60°C; 70 h; Product distribution / selectivity;
参考文献
BP CHEMICALS LIMITED
Patent: WO2003/82796 A1, 2003 ;
Location in patent: Page/Page column 9-13 ;
反应条件
pyridine in dichloromethane
T=0°C; 0.25 h;
参考文献
Fristrup, Peter; Jensen, Thomas; Hoppe, Jakob; Norrby, Per-Ola
Chemistry - A European Journal, 2006 , vol. 12, # 20 p. 5352 - 5360