反应条件
1: CuBr2; LiBr / ethyl acetate / 0.5 h / 90 °C 2: 600 mg / NaH / dimethylformamide / 3 h / 20 °C 3: 87 percent / diethyl ether / 4 h / 20 °C 4: 51 percent / pyridinium chlorochromate / CH2Cl2 / 4 h / 20 °C 5: 62 percent / m-chloroperbenzoic acid / CH2Cl2 / 3 h / -78 °C 6: 46 percent / NaHCO3 / CCl4 / 5 h / 80 °C View Scheme
参考文献
Boulin, Bertrand; Taran, Martine; Miguel, Bernadette Arreguy-San; Delmond, Bernard
Synthetic Communications, 2007 , vol. 37, # 15 p. 2579 - 2591