2,3,4-三甲氧基苯甲醇合成路线 （共 8 条）
反应条件
water; nickel dichloride; zinc in N,N-dimethyl-formamide 2 h; Ambient temperature;
参考文献
Baruah, Robindra N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, # 2 p. 182 - 183
反应条件
lithium aluminium tetrahydride
参考文献
Journal of the American Chemical Society, , vol. 76, p. 1776,1778
反应条件
potassium cyanide; sodium chloride in ice-water; dichloromethane; N,N-dimethyl-formamide
参考文献
Merck Patent Gesellschaft
Patent: US6534135 B1, 2003 ;
反应条件
oxygen; Nafion polymer anchored ruthenium oxide pyrochlore composite in acetone T=20°C; P=760.051 Torr; 7.5 h;
参考文献
Venkatesan; Kumar, A. Senthil; Zen
Tetrahedron Letters, 2008 , vol. 49, # 28 p. 4339 - 4341
反应条件
pyridine; thionyl chloride in dichloromethane 0.5 h;
参考文献
Hewgill, Frank R.; Slamet, Riskiono; Stewart, Jeffery M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3033 - 3042
参考文献
Ciba-Geigy Corporation
Patent: US5643878 A1, 1997 ;
反应条件
phosphorus tribromide in dichloromethane
T=0°C; 2 h; Inert atmosphere;
参考文献
Tanpure, Rajendra P.; Strecker, Tracy E.; Chaplin, David J.; Siim, Bronwyn G.; Trawick, Mary Lynn; Pinney, Kevin G.
Journal of Natural Products, 2010 , vol. 73, # 6 p. 1093 - 1101
反应条件
1: 95 percent / thionyl chloride, pyridine / CH2Cl2 / 0.5 h
2: 67 percent / toluene / 45 h / 60 °C
3: 82 percent / LiOMe / dimethylformamide; methanol / 4.5 h / 90 °C
View Scheme
参考文献
Hewgill, Frank R.; Slamet, Riskiono; Stewart, Jeffery M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3033 - 3042
