3,4,5-三乙酰氧基苯甲醛合成路线 （共 9 条）
反应条件
chloroform; sodium methylate
参考文献
Rosenmund; Zetzsche
Chemische Berichte, 1918 , vol. 51, p. 598
反应条件
pyridinium chlorochromate in dichloromethane
1 h;
参考文献
Schmidt, Ulrich; Wild, Jochen
Liebigs Annalen der Chemie, 1985 , # 9 p. 1882 - 1894
反应条件
triethylamine
T=20°C; 2 h;
参考文献
Zou, Hong Bin; Dong, Sheng Yi; Zhou, Chang Xin; Hu, Li Hong; Wu, Yi Hang; Li, Hai Bo; Gong, Jing Xu; Sun, Lian Li; Wu, Xiu Mei; Bai, Hua; Fan, Bo Tao; Hao, Xiao Jiang; Stoeckigt, Joachim; Zhao, Yu
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 6 p. 2060 - 2071
反应条件
1: 72 percent / BH3*Me2S / tetrahydrofuran / 20 °C
2: 70 percent / (COCl)2; DMSO; Et3N / CH2Cl2 / -78 - 20 °C
View Scheme
参考文献
Nielsen, Christian B.; Johnsen, Mette; Arnbjerg, Jacob; Pittelkow, Michael; McIlroy, Sean P.; Ogilby, Peter R.; Jorgensen, Mikkel
Journal of Organic Chemistry, 2005 , vol. 70, # 18 p. 7065 - 7079
反应条件
1: 85 percent / pyridinium chlorochromate / CH2Cl2 / 20 °C
2: 30 percent / AlCl3 / CH2Cl2 / 12 h / 20 °C
3: 75 percent / triethylamine / 2 h / 20 °C
View Scheme
参考文献
Zou, Hong Bin; Dong, Sheng Yi; Zhou, Chang Xin; Hu, Li Hong; Wu, Yi Hang; Li, Hai Bo; Gong, Jing Xu; Sun, Lian Li; Wu, Xiu Mei; Bai, Hua; Fan, Bo Tao; Hao, Xiao Jiang; Stoeckigt, Joachim; Zhao, Yu
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 6 p. 2060 - 2071
反应条件
1: 72 percent / LiAlH4 / tetrahydrofuran / Heating
2: 85 percent / pyridinium chlorochromate / CH2Cl2 / 20 °C
3: 30 percent / AlCl3 / CH2Cl2 / 12 h / 20 °C
4: 75 percent / triethylamine / 2 h / 20 °C
View Scheme
参考文献
Zou, Hong Bin; Dong, Sheng Yi; Zhou, Chang Xin; Hu, Li Hong; Wu, Yi Hang; Li, Hai Bo; Gong, Jing Xu; Sun, Lian Li; Wu, Xiu Mei; Bai, Hua; Fan, Bo Tao; Hao, Xiao Jiang; Stoeckigt, Joachim; Zhao, Yu
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 6 p. 2060 - 2071
反应条件
1: 30 percent / AlCl3 / CH2Cl2 / 12 h / 20 °C
2: 75 percent / triethylamine / 2 h / 20 °C
View Scheme
参考文献
Zou, Hong Bin; Dong, Sheng Yi; Zhou, Chang Xin; Hu, Li Hong; Wu, Yi Hang; Li, Hai Bo; Gong, Jing Xu; Sun, Lian Li; Wu, Xiu Mei; Bai, Hua; Fan, Bo Tao; Hao, Xiao Jiang; Stoeckigt, Joachim; Zhao, Yu
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 6 p. 2060 - 2071
反应条件
Pd-BaSO4; N,N-dimethyl-aniline; acetone
Hydrogenation;
参考文献
Sakurai; Tanabe
Yakugaku Zasshi, 1944 , vol. 64, # 8 p. 25
Chem.Abstr., 1951 , p. 5613
参考文献
Rosenmund; Zetzsche
Chemische Berichte, 1918 , vol. 51, p. 598
