1-(甲氧基甲基)-1H-苯并三唑合成路线 （共 14 条）
反应条件
n-butyllithium; zinc dibromide
1.) THF, -78 deg C, 1 h, 2.) THF, -78 deg C, 4 h; -78 deg C to room temperature, overnight, 3.) CHCl2CHCl2, 140 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Katritzky, Alan R.; Xie, Linghong; Serdyuk, Larisa
Journal of Organic Chemistry, 1996 , vol. 61, # 21 p. 7564 - 7570
反应条件
in diethyl ether; toluene
Heating;
参考文献
Katritzky, Alan R.; Rachwal, Stanislaw; Rachwal, Bogumila
Journal of Organic Chemistry, 1989 , vol. 54, # 26 p. 6022 - 6029
反应条件
n-butyllithium
1) THF, hexane, -78 deg C, 2h, 2a) THF, -78 to RT, 2b) RT, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Katritzky, Alan R.; Zhao, Xiaohong; Shcherbakova, Irina V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3295 - 3299
反应条件
n-butyllithium in tetrahydrofuran
-78 deg C, 30 min then r.t., 10 h;
参考文献
Katritzky, Alan R.; Zhang, Zhongxing; Lang, Hengyuan; Xie, Linghong
Heterocycles, 1998 , vol. 47, # 1 p. 187 - 194
