2-(氯甲基)-3-甲基萘合成路线 (共 4 条)
反应条件
sulfuryl dichloride; benzoyl chloride in tetrachloromethane
6 h; HeatingIrradiation;
参考文献
Abou-Teim, Omar; Goodland, Michael C.; McOmie, F. W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2659 - 2662
反应条件
thionyl chloride; zinc(II) chloride in 1,4-dioxane
0.666667 h;
参考文献
Ellingboe, John W.; Lombardo, Louis J.; Alessi, Thomas R.; Nguyen, Thomas T.; Guzzo, Frieda; et al.
Journal of Medicinal Chemistry, 1993 , vol. 36, # 17 p. 2485 - 2493
反应条件
1: DIBAL / tetrahydrofuran / 18 h / 0 - 20 °C
2: ZnCl2, SOCl2 / dioxane / 0.67 h
View Scheme
参考文献
Ellingboe, John W.; Lombardo, Louis J.; Alessi, Thomas R.; Nguyen, Thomas T.; Guzzo, Frieda; et al.
Journal of Medicinal Chemistry, 1993 , vol. 36, # 17 p. 2485 - 2493
反应条件
T=780°C; P=0.01 Torr; 1 h;
参考文献
Abou-Teim, Omar; Goodland, Michael C.; McOmie, F. W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2659 - 2662