(1S,3R)-3-氨基环戊羧酸合成路线 （共 12 条）
反应条件
hydrogen; palladium 10 on activated carbon in ethyl acetate T=20°C; 24 h;
参考文献
MERCK and CO., INC
Patent: WO2005/120505 A2, 2005 ;
Location in patent: Page/Page column 29-30 ;
WO 2005/120505 A2
反应条件
hydrogen; palladium 10 on activated carbon in ethyl acetate T=20°C; 24 h;
参考文献
Butora, Gabor; Guiadeen, Deodialsingh; Kothandaraman, Shankaran; MacCoss, Malcolm; Mills, Sander G.; Yang, Lihu
Patent: US2007/155731 A1, 2007 ;
Location in patent: Page/Page column 30 ;
US 20070155731 A1
反应条件
hydrogen; palladium on activated charcoal in acetic acid
参考文献
Evans, Chris; McCague, Ray; Roberts, Stanley M.; Sutherland, Alan G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 3 p. 656 - 657
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in water; acetonitrile
参考文献
Chenevert; Martin
Tetrahedron Asymmetry, 1992 , vol. 3, # 2 p. 199 - 200
反应条件
hydrogenchloride Heating;
参考文献
Evans, Chris; McCague, Ray; Roberts, Stanley M.; Sutherland, Alan G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 3 p. 656 - 657
反应条件
1: 91 percent / Dowex H+ resin / Heating 2: phosphate buffer / acetonitrile / 37 °C / pH 7.0, cholesterol esterase 3: 82 percent / NH3 / methanol 4: 92 percent / bis(trifluoroacetoxy)iodobenzene / acetonitrile; H2O View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 3, # 2 p. 199 - 200
反应条件
1: phosphate buffer / acetonitrile / 37 °C / pH 7.0, cholesterol esterase 2: 82 percent / NH3 / methanol 3: 92 percent / bis(trifluoroacetoxy)iodobenzene / acetonitrile; H2O View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 3, # 2 p. 199 - 200
反应条件
1: 82 percent / NH3 / methanol 2: 92 percent / bis(trifluoroacetoxy)iodobenzene / acetonitrile; H2O View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 3, # 2 p. 199 - 200
反应条件
1: 87 percent / tributyltin hydride, azobisisobutyronitrile / toluene / 5 h / Heating 2: 97 percent / aq. HCl / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 3 p. 656 - 657
反应条件
2: Br2, NaOH View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 5, # 3 p. 359 - 362
