1,1,1,3,3,3-六氟代-2-苯基-2-丙醇合成路线 （共 34 条）
反应条件
aluminium trichloride T=50 - 54°C; 5 h;
参考文献
Journal of Fluorine Chemistry, , vol. 24, p. 61 - 74
反应条件
sodium hydroxide in methanol; water Heating;
参考文献
Takechi, Naoto; Ait-Mohand, Samia; Medebielle, Maurice; Dolbier Jr., William R.
Tetrahedron Letters, 2002 , vol. 43, # 24 p. 4317 - 4319
反应条件
1: 94 percent / tetramethylammonium fluoride / 1,2-dimethoxy-ethane / -30 - 20 °C 2: 81 percent / hydrochloric acid / tetrahydrofuran; H2O / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 61, # 7 p. 1813 - 1819
反应条件
1: 92 percent / tetramethylammonium fluoride / 1,2-dimethoxy-ethane / -30 - 20 °C 2: 81 percent / hydrochloric acid / tetrahydrofuran; H2O / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 61, # 7 p. 1813 - 1819
反应条件
1: 82 percent / tetramethylammonium fluoride / 1,2-dimethoxy-ethane / -30 - 20 °C 2: 81 percent / hydrochloric acid / tetrahydrofuran; H2O / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 61, # 7 p. 1813 - 1819
反应条件
1: cesium fluoride / tetrahydrofuran / 96 h / 20 °C 2: ammonium chloride; water / diethyl ether View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 15 p. 7749 - 7753
参考文献
Journal of the American Chemical Society, , vol. 99, # 13 p. 4400 - 4404
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , # 4 p. 647 - 653
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 4 p. 686 - 692
参考文献
US6355849 B1, ;
Example 7 ;
反应条件
(i) SF4, (ii) NaF, CH2Cl2; Multistep reaction;
参考文献
Sheppard,W.A.
Journal of the American Chemical Society, 1965 , vol. 87, # 11 p. 2410 - 2420
