2,6-吡啶二羧酸单甲酯合成路线 （共 13 条）
反应条件
sodium hydroxide; phosphate buffer 13 h; Ambient temperaturepig liver esterase;
参考文献
Ager; Prakash
Synthetic Communications, 1995 , vol. 25, # 5 p. 739 - 742
参考文献
Ryan, Patrick E.; Canard, Gabriel; Koeller, Sylvain; Bocquet, Bernard; Piguet, Claude
Inorganic Chemistry, 2012 , vol. 51, # 18 p. 10012 - 10024
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran 4 h; Reflux;
参考文献
Tetrahedron, , vol. 67, # 44 p. 8458 - 8464
反应条件
1: 78 percent / H2SO4 / 48 h / 70 °C 2: 53 percent / KOH / methanol / 26 h / 0 - 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 11, # 4 p. 1109 - 1118
反应条件
sulfuric acid in water 1) 15 min, reflux, 2) RT, 10 h;
参考文献
Journal of Organic Chemistry, , vol. 46, # 24 p. 4914 - 4920
反应条件
1: 1.) n-butyllithium / 1.) THF, -89 deg C, 4 h, 2.) THF, from -89 deg C to RT 2: HCl / 24 h / Heating View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 186, # 2 p. 147 - 153
参考文献
Chemische Berichte, , vol. 86, p. 584,587
反应条件
1: SeO2; acetic acid 2: aqueous H2O2 View Scheme
参考文献
Chemische Berichte, , vol. 86, p. 584,587
反应条件
thionyl chloride in N,N-dimethyl-formamide T=60°C; Inert atmosphereCooling with ice;
参考文献
Macerata, Elena; Sansone, Francesco; Baldini, Laura; Ugozzoli, Franco; Brisach, Frederic; Haddaoui, Jaouad; Hubscher-Bruder, Veronique; Arnaud-Neu, Francoise; Mariani, Mario; Ungaro, Rocco; Casnati, Alessandro
European Journal of Organic Chemistry, 2010 , # 14 p. 2675 - 2686
参考文献
Nakahara, Satoshi; Kusano, Miyako; Fujioka, Shozo; Shimada, Atsumi; Kimura, Yasuo
Bioscience, Biotechnology and Biochemistry, 2004 , vol. 68, # 1 p. 257 - 259
