1,3,5-三异丙基苯合成路线 （共 123 条）
反应条件
titanium(IV) isopropylate; chloro-trimethyl-silane; magnesium in tetrahydrofuran T=50°C; Inert atmosphere;
参考文献
Organic Letters, , vol. 13, # 10 p. 2626 - 2629
反应条件
triethylamine; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane T=100°C; 6 h;
参考文献
Murata, Miki; Sambommatsu, Tomoko; Watanabe, Shinji; Masuda, Yuzuru
Synlett, 2006 , # 12 p. 1867 - 1870
反应条件
toluene-4-sulfonic acid in neat (no solvent) T=60 - 140°C; 20 h; Green chemistry; regioselective reaction;
参考文献
Gao, Qi; Bao, Fang-Ping; Feng, Xiao-Jing; Pan, Ying-Ming; Wang, Heng-Shan; Li, Dian-Peng
Arkivoc, 2013 , vol. 2013, # 3 p. 49 - 60
反应条件
1: 2-bromo-1,3,5-triisopropylbenzene With 1,2-dibrom-methane; magnesium in tetrahydrofuran 3.5 h; Heating; 2: 2,4,6-tribromo-1-iodobenzene in tetrahydrofuran 5 h; Heating; Further stages.;
参考文献
Journal of the American Chemical Society, , vol. 124, # 22 p. 6252 - 6253
反应条件
sulfuric acid T=30 - 40°C;
参考文献
Journal of the American Chemical Society, , vol. 65, p. 320
反应条件
aluminium trichloride T=25°C; Alkylation; 0.75 h;
参考文献
Ghiaci; Asghari
Synthetic Communications, 1998 , vol. 28, # 12 p. 2213 - 2220
反应条件
potassium phosphate; palladium diacetate in methanol; benzene T=40°C; 18 h;
参考文献
Demchuk, Oleg M.; Yoruk, Bilge; Blackburn, Tom; Snieckus, Victor
Synlett, 2006 , # 18 p. 2908 - 2913
反应条件
indium(III) chloride; 2-iodophenol in chlorobenzene 24 h; Reflux; regioselective reaction;
参考文献
Xu, Yan-Li; Pan, Ying-Ming; Wu, Qiang; Wang, Heng-Shan; Liu, Pei-Zhen
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8472 - 8476
反应条件
1: meta-dibromobenzene With n-butyllithium in diethyl ether T=-78 - 20°C; 0.0833333 h; Inert atmosphere; 2: TripB(OMe)2 in tetrahydrofuran; diethyl ether T=20°C; 2 h; Inert atmosphere;
参考文献
Pron, Agnieszka; Zhou, Gang; Norouzi-Arasi, Hassan; Baumgarten, Martin; Muellen, Klaus
Organic Letters, 2009 , vol. 11, # 16 p. 3550 - 3553
反应条件
aluminosilicate T=70°C; effect of the composition and amount of catalysts, reaction time and temperature; Rate constantProduct distribution;
参考文献
Journal of applied chemistry of the USSR, , vol. 58, # 4 pt 1 p. 754 - 760
