2,3-二甲氧基苯甲酰氯合成路线 （共 40 条）
反应条件
1.1: tetrahydrofuran / 5 h / -10 °C
1.2: 54 percent / Et3N / tetrahydrofuran / 0.5 h / -10 °C
2.1: 41 percent / Me6Sn2 / 1,2-dichloro-benzene / 4 h / Irradiation
View Scheme
参考文献
Taniguchi, Tsuyoshi; Iwasaki, Keiko; Uchiyama, Masahiko; Tamura, Osamu; Ishibashi, Hiroyuki
Organic Letters, 2005 , vol. 7, # 20 p. 4389 - 4390
反应条件
1: CH2Cl2 / 20 h / 20 °C
2: SOCl2 / 7 h / 20 °C
View Scheme
参考文献
Denieul, Marie-Pierre; Skrydstrup, Troels
Tetrahedron Letters, 1999 , vol. 40, # 26 p. 4901 - 4904
参考文献
Chew, Warren; Hynes, Rosemary C.; Harpp, David N.
Journal of Organic Chemistry, 1993 , vol. 58, # 16 p. 4398 - 4404
反应条件
in toluene
T=20°C; 1 h;
参考文献
Rudrawar, Santosh; Kondaskar, Atul; Chakraborti, Asit K.
Synthesis, 2005 , # 15 art. no. Z05105SS, p. 2521 - 2526
反应条件
aluminium trichloride in dichloromethane
T=20°C; 15 h;
参考文献
Helesbeux, Jean-Jacques; Duval, Olivier; Dartiguelongue, Caroline; Seraphin, Denis; Oger, Jean-Michel; Richomme, Pascal
Tetrahedron, 2004 , vol. 60, # 10 p. 2293 - 2300
参考文献
Woodruff
Journal of the American Chemical Society, 1942 , vol. 64, p. 2859,2860
反应条件
beim Erwaermen des erhaltenen Reaktionsprodukts mit Essigsaeure,HCl und H2O;
参考文献
Senoh; Sakan
Nippon Kagaku Zasshi, 1953 , vol. 74, p. 654
Chem.Abstr., 1954 , p. 12027
反应条件
beim Erwaermen des erhaltenen Reaktionsprodukts mit wss.H2SO4;
参考文献
Ahluwalia et al.
Proceedings - Indian Academy of Sciences, Section A, 1953 , # 38 p. 480,490
反应条件
1: 86 percent / AlCl3 / CH2Cl2 / 15 h / 20 °C
2: 93 percent / pyridine; aq. tetramethylammonium hydroxide / 4 h / Heating
3: 95 percent / aq. HI; phenol / 24 h / Heating
4: 13 percent / aq. KOH / 16 h / 20 °C
View Scheme
参考文献
Helesbeux, Jean-Jacques; Duval, Olivier; Dartiguelongue, Caroline; Seraphin, Denis; Oger, Jean-Michel; Richomme, Pascal
Tetrahedron, 2004 , vol. 60, # 10 p. 2293 - 2300
反应条件
in tetrahydrofuran
1) 1h, -100 deg C, 2) allowed up to 25 deg C over 2 h;
参考文献
Parham; Bradsher; Edgar
Journal of Organic Chemistry, 1981 , vol. 46, # 6 p. 1057 - 1061
