4,6-二甲氧基异邻苯二甲酸合成路线 （共 9 条）
反应条件
hydrogen iodide T=130°C;
参考文献
Jois; Manjunath; Siddappa
J. Mysore Univ., 1932 , vol. 6, p. 96
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Birkinshaw; Raistrick
Biochemical Journal, 1932 , vol. 26, p. 441,444, 445
反应条件
sodium hydroxide in methanol; water
4 h; Heating;
参考文献
Yuan, Lihua; Sanford, Adam R.; Feng, Wen; Zhang, Aimin; Zhu, Jin; Zeng, Huaqiang; Yamato, Kazuhiro; Li, Minfeng; Ferguson, Joseph S.; Gong, Bing
Journal of Organic Chemistry, 2005 , vol. 70, # 26 p. 10660 - 10669
反应条件
1: anschliessend mit Hexamethylentetramin in CHCl3 und Erhitzen des Reaktionsprodukts mit H2O
2: aqueous KMnO4
View Scheme
参考文献
Wood et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 2992
反应条件
1: sulfuric acid / Heating
2: 93 percent / K2CO3 / acetone / 72 h / Heating
3: 92.1 percent / NaOH / methanol; H2O / 4 h / Heating
View Scheme
参考文献
Yuan, Lihua; Sanford, Adam R.; Feng, Wen; Zhang, Aimin; Zhu, Jin; Zeng, Huaqiang; Yamato, Kazuhiro; Li, Minfeng; Ferguson, Joseph S.; Gong, Bing
Journal of Organic Chemistry, 2005 , vol. 70, # 26 p. 10660 - 10669
参考文献
Dallacker,F.; Korb,W.
Justus Liebigs Annalen der Chemie, 1966 , vol. 694, p. 98 - 109
参考文献
Birkinshaw; Raistrick
Biochemical Journal, 1932 , vol. 26, p. 441,444, 445
参考文献
Spaeth et al.
Chemische Berichte, 1931 , vol. 64, p. 2203,2208
参考文献
Eijkman; Bergema; Henrard
Chem. Zentralbl., 1905 , vol. 76, # I p. 815
反应条件
thionyl chloride in N,N-dimethyl-formamide
Heating;
参考文献
Wu, Zong-Quan; Shao, Xue-Bin; Li, Chuang; Hou, Jun-Li; Wang, Kui; Jiang, Xi-Kui; Li, Zhan-Ting
Journal of the American Chemical Society, 2005 , vol. 127, # 49 p. 17460 - 17468
