(3E)-3-己烯-1,6-二醇合成路线 （共 10 条）
反应条件
1: PBr3, Py 3: H2 / PtO2 View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 6, p. 402 - 405
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=20°C; Reduction; 2 h;
参考文献
Hoppen, Sabine; Baeurle, Stefan; Koert, Ulrich
Chemistry - A European Journal, 2000 , vol. 6, # 13 p. 2382 - 2396
反应条件
lithium aluminium tetrahydride in diethyl ether
0.5 h; Ambient temperature;
参考文献
Cantin, Michel; Xu, Yao-Chang; Deslongchamps, Pierre
Canadian Journal of Chemistry, 1990 , vol. 68, # 12 p. 2144 - 2152
反应条件
lithium aluminium tetrahydride; hydrogen cation in methanol
参考文献
Lipshutz, Brace H.; James, Brian; Vance, Shelly; Cairico, Isaac
Tetrahedron Letters, 1997 , vol. 38, # 5 p. 753 - 756
反应条件
1: HCl
2: LiAlH4
View Scheme
参考文献
Burger,A.; Bedford,G.R.
Journal of Medicinal Chemistry, 1963 , vol. 6, p. 402 - 405
参考文献
Raphael; Roxburgh
Journal of the Chemical Society, 1952 , p. 3875
反应条件
1: sulfuric acid; methanol
2: sodium; liquid ammonia
View Scheme
参考文献
Raphael; Roxburgh
Journal of the Chemical Society, 1952 , p. 3875
反应条件
1: 91 percent / Et3N / CH2Cl2
2: 80 percent / NaI / acetone
View Scheme
参考文献
Wittig,G.; Wingler,F.
Chemische Berichte, 1964 , vol. 97, p. 2146 - 2164
反应条件
1H-imidazole in N,N-dimethyl-formamide
T=20°C; 5 h; Inert atmosphere;
参考文献
Wang, Cuihua; Barluenga, Sofia; Koripelly, Girish K.; Fontaine, Jean-Gonzague; Chen, Ruihong; Yu, Jin-Chen; Shen, Xiaodong; Chabala, John C.; Heck, James V.; Rubenstein, Allan; Winssinger, Nicolas
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 14 p. 3836 - 3840
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane
15 h;
参考文献
McNaughton, Brian R.; Bucholtz, Kevin M.; Camaano-Moure, Ana; Miller, Benjamin L.
Organic Letters, 2005 , vol. 7, # 4 p. 733 - 736
