2-(2-吡啶)苯并噻唑合成路线 （共 40 条）
反应条件
trichloroisocyanuric acid in 2-methyl tetrahydrofuran
T=20°C; 5 h;
参考文献
Xiao, Hui-Long; Chen, Jiu-Xi; Liu, Miao-Chang; Zhu, Dong-Jian; Ding, Jin-Chang; Wu, Hua-Yue
Chemistry Letters, 2009 , vol. 38, # 2 p. 170 - 171
反应条件
{PdCl2[(t-Bu)2PCl]2}; Cu[9,9-dimethyl-4,5-bis(diphenylphosphine)xanthene]I; caesium carbonate in toluene
T=100°C; Inert atmosphere;
参考文献
Huang, Jinkun; Chan, Johann; Chen, Ying; Borths, Christopher J.; Baucom, Kyle D.; Larsen, Robert D.; Faul, Margaret M.
Journal of the American Chemical Society, 2010 , vol. 132, # 11 p. 3674 - 3675
反应条件
dipotassium peroxodisulfate; FeCl3·6H2O in water; dimethyl sulfoxide
T=100°C; 12 h;
参考文献
Wang, Jian; Zhang, Xiao-Zhuan; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron, 2014 , vol. 70, # 2 p. 245 - 250
反应条件
1: With copper(l) iodide; Na2S*9H2O in N,N-dimethyl-formamide
T=80°C; 12 h;
2: With hydrogenchloride in N,N-dimethyl-formamide
T=20°C;
参考文献
Ma, Dawei; Xue, Peng; Jiang, Yongwen; Xie, Siwei; Zhang, Xiaojing; Dong, Jinhua
Angewandte Chemie, International Edition, 2009 , vol. 48, # 23 p. 4222 - 4225
反应条件
Lawesson's reagent
T=190°C; 0.0166667 h; microwave irradiation;
参考文献
Seijas, Julio A.; Vazquez-Tato, M. Pilar; Carballido-Reboredo, M. Raquel; Crecente-Campo, Jose; Romar-Lopez, Lucia
Synlett, 2007 , # 2 p. 313 - 317
反应条件
sulfur in neat (no solvent)
T=120°C; 24 h; Sealed tubeInert atmosphere;
参考文献
Nguyen, Thanh Binh; Ermolenko, Ludmila; Al-Mourabit, Ali
Organic Letters, 2013 , vol. 15, # 16 p. 4218 - 4221
反应条件
tetrabutylammomium bromide; silver(I) acetate; palladium diacetate; potassium carbonate in N,N-dimethyl-formamide
T=120°C; 18 h; Molecular sieveInert atmosphere;
参考文献
Saha, Debasree; Adak, Laksmikanta; Ranu, Brindaban C.
Tetrahedron Letters, 2010 , vol. 51, # 42 p. 5624 - 5627
反应条件
toluene-4-sulfonic acid in PEG-200/400
0.166667 h; Microwave irradiation;
参考文献
Deligeorgiev, Todor G.; Kaloyanova, Stefka; Vasilev, Aleksey; Vaquero, Juan J.
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 11 p. 2292 - 2302
反应条件
{PdCl2[(t-Bu)2PCl]2}; Cu[9,9-dimethyl-4,5-bis(diphenylphosphine)xanthene]I; caesium carbonate in toluene
T=100°C; Inert atmosphere;
参考文献
Huang, Jinkun; Chan, Johann; Chen, Ying; Borths, Christopher J.; Baucom, Kyle D.; Larsen, Robert D.; Faul, Margaret M.
Journal of the American Chemical Society, 2010 , vol. 132, # 11 p. 3674 - 3675
反应条件
magnesium sulfate; copper(l) chloride in dimethyl sulfoxide
T=110°C; 6 h;
参考文献
Park, Namjin; Heo, Yumi; Kumar, Manian Rajesh; Kim, Yong; Song, Kwang Ho; Lee, Sunwoo
European Journal of Organic Chemistry, 2012 , # 10 p. 1984 - 1993
