反应条件
potassium tert-butylate; triethylamine
1.) CH2Cl2, -15 deg C, 2 h, irradiation, 2.) reflux, 1 h, 3.) THF, t-BuOH, 0 deg C; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Block,E.; Aslam,M.
Journal of the American Chemical Society, 1983 , vol. 105, p. 6165