4'-甲氧基-4-(对甲氧基苯基)苯丁酮合成路线 (共 3 条)
反应条件
aluminium trichloride in 1,2-dichloro-ethane
0.0833333 h;
参考文献
Kogan, Timothy P.; Dupre, Brian; Bui, Huong; McAbee, Kathy L.; Kassir, Jamal M.; Scott, Ian L.; Hu, Xin; Vanderslice, Peter; Beck, Pamela J.; Dixon, Richard A. F.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 7 p. 1099 - 1111
反应条件
1: thionyl chloride / 20 - 65 °C
2: 82 percent / AlCl3 / 1,2-dichloro-ethane / 0.08 h
View Scheme
参考文献
Kogan, Timothy P.; Dupre, Brian; Bui, Huong; McAbee, Kathy L.; Kassir, Jamal M.; Scott, Ian L.; Hu, Xin; Vanderslice, Peter; Beck, Pamela J.; Dixon, Richard A. F.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 7 p. 1099 - 1111
反应条件
triethylsilane; boron trifluoride diethyl etherate; trifluoroacetic acid in dichloromethane
2 h; Ambient temperature;
参考文献
Kogan, Timothy P.; Dupre, Brian; Bui, Huong; McAbee, Kathy L.; Kassir, Jamal M.; Scott, Ian L.; Hu, Xin; Vanderslice, Peter; Beck, Pamela J.; Dixon, Richard A. F.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 7 p. 1099 - 1111