1-氯-2,3,4,5-四氟-6-(三氟甲基)苯合成路线 （共 8 条）
反应条件
1: steam / 330 °C / Leiten ueber Aluminiumoxid 2: hydrogen / 280 °C / Leiten ueber Palladium/Kohle View Scheme
参考文献
Pummer; Florin; Wall
Journal of Research of the National Bureau of Standards (United States), 1959 , vol. 62, p. 113
反应条件
palladium on activated charcoal T=290°C;
参考文献
Florin et al.
Journal of Research of the National Bureau of Standards (United States), 1959 , vol. 62, p. 119,121
反应条件
1: steam / 330 °C / Leiten ueber Aluminiumoxid 2: steam; Al2O3 / 330 °C View Scheme
参考文献
Pummer; Florin; Wall
Journal of Research of the National Bureau of Standards (United States), 1959 , vol. 62, p. 113
反应条件
1: steam / 330 °C / Leiten ueber Aluminiumoxid 2: hydrogen / 280 °C / Leiten ueber Palladium/Kohle 3: fuming sulfuric acid; iodine View Scheme
参考文献
Journal of Research of the National Bureau of Standards (United States), , vol. 62, p. 113
反应条件
bromine trifluoride
T=100°C; anschliessend Erhitzen mit SbF5 auf 120grad und Kochen des Reaktionsprodukts mit Zinkstaub und Aethanol;
参考文献
McBee; Lindgren; Ligett
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 378,379
Show Details
Purdue Research Found.
Patent: US2459779 , 1945 ;
Full Text Show Details
Florin; Pummer; Wall
Journal of Research of the National Bureau of Standards (United States), 1959 , vol. 62, p. 107,110
反应条件
hexaethylguanidinium chloride; sodium bromide
T=140 - 145°C; 7 h; Product distribution; Further Variations:Reagents;
参考文献
Shipilov; Zolotkova; Igumnov
Russian Journal of Organic Chemistry, 2004 , vol. 40, # 8 p. 1117 - 1120
反应条件
hexaethylguanidinium chloride; sodium chloride
T=140 - 145°C; 7 h; Product distribution; Further Variations:Reagents;
参考文献
Shipilov; Zolotkova; Igumnov
Russian Journal of Organic Chemistry, 2004 , vol. 40, # 8 p. 1117 - 1120
反应条件
steam
T=330°C; Leiten ueber Aluminiumoxid;
参考文献
Pummer; Florin; Wall
Journal of Research of the National Bureau of Standards (United States), 1959 , vol. 62, p. 113
