N,N-双-(2-羟乙基)-对甲苯磺酰胺合成路线 （共 16 条）
反应条件
triethylamine in dichloromethane T=20°C; 4 h;
参考文献
Yar, Muhammad; Mushtaq, Nafeesa; Afzal, Sadia; Khan, Abdul Samad; Khan, Islam Ullah; Akhter, Muhammad Nadeem; Zareen, Seema; Shahzad, Sohail Anjum; Khan, Zulfiqar Ali; Raza Naqvi, Syed Ali; Mahmood, Nasir; Tahir, Lubna; Saleem, Muhammad
Asian Journal of Chemistry, 2013 , vol. 25, # 13 p. 7297 - 7304
反应条件
Amberlist-15 in methanol T=20°C; Substitution; 12 h;
参考文献
Arisawa, Mitsuhiro; Kato, Chiaki; Kaneko, Hiroaki; Nishida, Atsushi; Nakagawa, Masako
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 12 p. 1873 - 1876
反应条件
sodium hydroxide; benzene
参考文献
Ukrainskii Khimicheskii Zhurnal (Russian Edition), , vol. 25, p. 615
Chem.Abstr., , p. 12041
US2727004 , ;
参考文献
US1859527 , ;
DE520156 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 651
参考文献
Journal of the Chemical Society, , p. 1303
反应条件
thionyl chloride T=110°C; 1 h;
参考文献
Al-Rashood; Madani; Ginawi; Ashraf; El-Obeid
Arzneimittel-Forschung/Drug Research, 1990 , vol. 40, # 11 p. 1242 - 1245
反应条件
sulfuric acid T=170 - 180°C;
参考文献
ICI
Patent: DE520156 , 1928 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 651
Full Text Show Details
ICI
Patent: US1859527 , 1927 ;
反应条件
1: 100 percent / Et3N / CH2Cl2 / 0.25 h / -10 °C 2: 53 percent / sodium azide, Aliquat 336 / H2O / 2 h / Heating 3: 66 percent / LiAlH4 / tetrahydrofuran / 0.5 h / 10 °C View Scheme
参考文献
Bartsch, Richard A.; Chapoteau, Eddy; Czech, Bronislaw P.; Krzykawski, Jan; Kumar, Anand; Robison, Thomas W.
Journal of Organic Chemistry, 1994 , vol. 59, # 3 p. 616 - 621
反应条件
1: 100 percent / Et3N / CH2Cl2 / 0.25 h / -10 °C 2: 53 percent / sodium azide, Aliquat 336 / H2O / 2 h / Heating View Scheme
参考文献
Yar, Muhammad; Mushtaq, Nafeesa; Afzal, Sadia; Khan, Abdul Samad; Khan, Islam Ullah; Akhter, Muhammad Nadeem; Zareen, Seema; Shahzad, Sohail Anjum; Khan, Zulfiqar Ali; Raza Naqvi, Syed Ali; Mahmood, Nasir; Tahir, Lubna; Saleem, Muhammad
Asian Journal of Chemistry, 2013 , vol. 25, # 13 p. 7297 - 7304
参考文献
Vaidya, Bikas; Zak, Jerzy; Bastiaans, Glenn J.; Porter, Marc D.; Hallman, Johnny L.; Nabulsi, Nabeel A. R.; Utterback, Marty D.; Strzelbicka, Bozena; Bartsch, Richard A.
Analytical Chemistry, 1995 , vol. 67, # 22 p. 4101 - 4111
