3,4-(亚甲二氧基)甲苯合成路线 （共 45 条）
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in methanol T=20°C; P=760.051 Torr; 0.5 h;
参考文献
Xing, Lixin; Wang, Xinyan; Cheng, Chuanjie; Zhu, Rui; Liu, Bo; Hu, Yuefei
Tetrahedron, 2007 , vol. 63, # 38 p. 9382 - 9386
反应条件
caesium carbonate in acetonitrile 4 h; Reflux;
参考文献
Tuley, Alfred; Wang, Yane-Shih; Fang, Xinqiang; Kurra, Yadagiri; Rezenom, Yohannes H.; Liu, Wenshe R.
Chemical Communications, 2014 , vol. 50, # 20 p. 2673 - 2675
反应条件
hydrogen; palladium on activated charcoal in ethanol P=2585.7 Torr; 6 h; Ambient temperature;
参考文献
Meyers, A. I.; Himmelsbach, Richard J.; Reuman, Michael
Journal of Organic Chemistry, 1983 , vol. 48, # 22 p. 4053 - 4058
反应条件
cis-IrCl(CO)(PPh3)2; hydrazine hydrate; potassium hydroxide in methanol T=160°C; Wolff-Kishner Reduction; 3 h; Sealed tube; Reagent/catalystSolventTemperature;
参考文献
Huang, Jian-Lin; Dai, Xi-Jie; Li, Chao-Jun
European Journal of Organic Chemistry, 2013 , # 29 p. 6496 - 6500
反应条件
sodium hydroxide in CH12Cl2; hexane
参考文献
Advanced Life Sciences, Inc.
Patent: US2004/77554 A1, 2004 ;
反应条件
sodium tetrahydroborate; NiII chloride hexahydrate in tetrahydrofuran; methanol T=20°C; 0.5 h;
参考文献
Khurana, Jitender M.; Magoo, Devanshi
Synthetic Communications, 2010 , vol. 40, # 19 p. 2908 - 2913
反应条件
5-fluoro-1-(tetrahydro-furan-2-yl)-uracil in 1,4-dioxane T=330°C; 5 h; Gas phase; Product distribution / selectivity;
参考文献
RHODIA CHIMIE
Patent: US2008/21228 A1, 2008 ;
Location in patent: Page/Page column 5 ;
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; methyl-ethyl phosphite; tri-iso-propylsilane in ethylcyclohexane T=130°C; 15 h; Inert atmosphere;
参考文献
Tobisu, Mamoru; Nakamura, Ryo; Kita, Yusuke; Chatani, Naoto
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 3 p. 582 - 587
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene Decomposition; 4 h; Heating;
参考文献
Organic Letters, , vol. 2, # 3 p. 307 - 310
反应条件
caesium carbonate in N,N-dimethyl-formamide T=20 - 110°C;
参考文献
Tetrahedron, , vol. 59, # 24 p. 4383 - 4387
