2-甲基-2-丙基(1-羟基-2-氧代-3-氮杂环丁基)氨基甲酸酯合成路线 （共 3 条）
反应条件
hydrogen; palladium on activated charcoal in methanol P=760 Torr; 0.75 h;
参考文献
Mattingly, Phillip G.; Miller, Marvin J.
Journal of Organic Chemistry, 1980 , vol. 45, # 3 p. 410 - 415
反应条件
1: 79.5 percent / dicyclohexylcarbodiimide / tetrahydrofuran; H2O / 3 h / pH 4.5 2: 62 percent / Ph3P, diethyl azodicarboxylate / tetrahydrofuran / 6 h / 50 °C 3: 100 percent / H2 / 10percent Pd/C / methanol / 0.75 h / 760 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 3 p. 410 - 415
反应条件
1: 62 percent / Ph3P, diethyl azodicarboxylate / tetrahydrofuran / 6 h / 50 °C 2: 100 percent / H2 / 10percent Pd/C / methanol / 0.75 h / 760 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 3 p. 410 - 415
