2,3-二氢-1,4-乙桥喹喔啉合成路线 （共 7 条）
反应条件
1: n-BuLi / hexane; tetrahydrofuran / 0.17 h / 20 °C 2: air / hexane; tetrahydrofuran / 1 h View Scheme
参考文献
Gall', A. A.; Trachum, A. S.; Romantsev, V. A.; Shishkin, G. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 6 p. 626 - 630
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , vol. 27, # 6 p. 798 - 803
反应条件
n-butyllithium in tetrahydrofuran; hexane T=20°C; 0.166667 h;
参考文献
Gall', A. A.; Trachum, A. S.; Romantsev, V. A.; Shishkin, G. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 6 p. 626 - 630
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , vol. 27, # 6 p. 798 - 803
反应条件
1: n-BuLi / hexane; tetrahydrofuran / 0.17 h / 20 °C 2: hexane; tetrahydrofuran / 0.5 h / 20 °C View Scheme
参考文献
Gall', A. A.; Trachum, A. S.; Romantsev, V. A.; Shishkin, G. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 6 p. 626 - 630
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , vol. 27, # 6 p. 798 - 803
反应条件
in diethyl ether T=20°C; 24 h;
参考文献
Luk'yanchuk, N. P.; Sagalaeva, N. I.; Soboleva, V. K.; Shishkin, G. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 7 p. 792 - 798
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 7 p. 966 - 972
反应条件
potassium tert-butylate in tert-butyl alcohol
Heating;
参考文献
Doronina, S. O.; Gall', A. A.; Shishkin, G. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 8 p. 917 - 920
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 8 p. 1091 - 1094
反应条件
hydrogen bromide
T=100°C; 15 h; other concentration of HBr, various reagents (LiBr, H2SO4, HClO4, polyphosphoric acid), various time; Equilibrium constantProduct distribution;
参考文献
Shishkin, G. V.; Gall, A. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 6 p. 648 - 653
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , # 6 p. 831 - 836
反应条件
hydrogen bromide
T=100°C; 15 h; other concentration of HBr, various reagents (LiBr, H2SO4, HClO4, polyphosphoric acid), various time; Equilibrium constantProduct distribution;
参考文献
Shishkin, G. V.; Gall, A. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 6 p. 648 - 653
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , # 6 p. 831 - 836
