反式-(4-甲基-环己基)-乙酸合成路线 （共 7 条）
反应条件
carbon monoxide; palladium diacetate; 1,4-di(diphenylphosphino)-butane in ethylene glycol dimethyl ether
T=150°C; P=5168 Torr; 16 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ali, Bassam El; Alper, Howard
Journal of Organic Chemistry, 1993 , vol. 58, # 13 p. 3595 - 3596
反应条件
sulfuric acid in acetic acid
参考文献
Carr; Gray; McDonnell
Molecular crystals and liquid crystals, 1982 , vol. 97, # 1-4 p. 13 - 28
反应条件
1: 100 percent / SOCl2
2: 91 percent / LiAlH4 / diethyl ether
3: 76 percent / HBr, aq/H2SO4
4: 93 percent / dimethylsulfoxide
5: 78 percent / H2SO4 / acetic acid
View Scheme
参考文献
Carr; Gray; McDonnell
Molecular crystals and liquid crystals, 1982 , vol. 97, # 1-4 p. 13 - 28
反应条件
1: 76 percent / HBr, aq/H2SO4
2: 93 percent / dimethylsulfoxide
3: 78 percent / H2SO4 / acetic acid
View Scheme
参考文献
Carr; Gray; McDonnell
Molecular crystals and liquid crystals, 1982 , vol. 97, # 1-4 p. 13 - 28
反应条件
1: 91 percent / LiAlH4 / diethyl ether
2: 76 percent / HBr, aq/H2SO4
3: 93 percent / dimethylsulfoxide
4: 78 percent / H2SO4 / acetic acid
View Scheme
参考文献
Carr; Gray; McDonnell
Molecular crystals and liquid crystals, 1982 , vol. 97, # 1-4 p. 13 - 28
反应条件
1: 93 percent / dimethylsulfoxide
2: 78 percent / H2SO4 / acetic acid
View Scheme
参考文献
Carr; Gray; McDonnell
Molecular crystals and liquid crystals, 1982 , vol. 97, # 1-4 p. 13 - 28
反应条件
sulfuric acid
Heating;
参考文献
Gerlach,H.
Helvetica Chimica Acta, 1966 , vol. 49, p. 1291 - 1302
