4,5-二氢-2-苯基恶唑合成路线 (共 96 条)
反应条件
sodium nitrite in water
T=25°C; 0.0333333 h;
参考文献
Loeppky, Richard N.; Cui, Wenge
Tetrahedron Letters, 1998 , vol. 39, # 14 p. 1845 - 1848
反应条件
sodium nitrite in water; acetic acid
T=25°C; 0.0333333 h;
参考文献
Loeppky, Richard N.; Cui, Wenge
Tetrahedron Letters, 1998 , vol. 39, # 14 p. 1845 - 1848
反应条件
sodium nitrite in water
T=25°C; 0.0333333 h;
参考文献
Loeppky, Richard N.; Cui, Wenge
Tetrahedron Letters, 1998 , vol. 39, # 14 p. 1845 - 1848
反应条件
(i), (ii) Na2CO3, D2O; Multistep reaction;
参考文献
Deslongchamps,P. et al.
Canadian Journal of Chemistry, 1975 , vol. 53, p. 2791 - 2807
反应条件
1: 56 percent / NBS / AIBN / CCl4 / 12 h / Heating
2: 1.) BuLi / 1.) THF, -18 deg C, 15 min, 2.) room temp., overnight
View Scheme
参考文献
Kashima, Choji; Arao, Hideki
Synthesis, 1989 , # 11 p. 873 - 874
反应条件
sodium hydroxide; sodium hypochlorite; tetra(n-butyl)ammonium hydrogensulfate
1.) ethyl acetate, water, 12 h, room temp.; 2.) CH3OH, 5 h, room temp.; Yield given. Multistep reaction;
参考文献
Levin, Jeremy I.; Weinreb, Steven M.
Tetrahedron Letters, 1982 , vol. 23, # 23 p. 2347 - 2350