4,5-二氢-2-苯基恶唑合成路线 (共 96 条)
反应条件
highly sulfonated carbon solid acid (CH0.43O0.65S0.22) 0.666667 h; Sonication;
参考文献
Wang, Ling; Guo, Bin; Li, Hong-Xi; Li, Qi; Li, Hai-Yan; Lang, Jian-Ping
Dalton Transactions, 2013 , vol. 42, # 44 p. 15570 - 15580
反应条件
copper(II) bis(trifluoromethanesulfonate); diisopropyl-carbodiimide in 1,4-dioxane 5 h; Heating;
参考文献
Crosignani, Stefano; Young, Abigail C.; Linclau, Bruno
Tetrahedron Letters, 2004 , vol. 45, # 52 p. 9611 - 9615
反应条件
n-butyllithium; naphthalenyllithium; ortho-dibromobenzene in tetrahydrofuran; hexane 1.) -78 deg C, 8 h, 2.) -78 deg C to r.t.;
参考文献
Barluenga, Jose; Montserrat, Javier M.; Florez, Josefa
Journal of Organic Chemistry, 1993 , vol. 58, # 22 p. 5976 - 5980
反应条件
KO2 in acetonitrile T=20°C; 72 h;
参考文献
Kim, Yong Il; Kim, Yong Hae
Synlett, 1997 , vol. 1997, # 11 p. 1324 - 1326
反应条件
1,1,3,3-tetraphenyl-2-oxa-1,3-phospholanium bis(trifluoromethanesulfonate) in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Petersson, Maria J.; Jenkins, Ian D.; Loughlin, Wendy A.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 4 p. 739 - 746
反应条件
TBBDA T=20°C; 0.0833333 h; Neat (no solvent);
参考文献
Ghorbani-Vaghei; Akbari-Dadamahaleh; Amiri
Journal of the Iranian Chemical Society, 2010 , vol. 7, # 2 p. 301 - 307
反应条件
palladium diacetate; magnesium sulfate; triethylamine; di-(1-adamantyl)-n-butylphosphine in toluene T=110°C; P=7500.75 Torr; 16 h; AutoclaveInert atmosphere; Reagent/catalystSolvent;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Neumann, Stephan; Beller, Matthias
Chemistry - A European Journal, 2012 , vol. 18, # 43 p. 13619 - 13623
反应条件
triethylamine in 1,2-dichloro-ethane
参考文献
US2004/82553 A1, ;
US 20040082553 A1
反应条件
1: 3 - 4 h; Heating; 2: With boric acid in toluene T=130°C; 3: With CaO T=280°C; 3 h;
参考文献
Ilkgul, Baris; Gunes, Deniz; Sirkecioglu, Okan; Bicak, Niyazi
Tetrahedron Letters, 2010 , vol. 51, # 40 p. 5313 - 5315
反应条件
1: benzyl alcohol With iodine; potassium carbonate in tert-butyl alcohol T=70°C; 8 h; 2: ethanolamine in tert-butyl alcohol T=70°C; 18 h;
参考文献
Ishihara, Midori; Togo, Hideo
Tetrahedron, 2007 , vol. 63, # 6 p. 1474 - 1480