1-(4-甲基苯基)-3-丁烯-1-基乙酸酯合成路线 （共 10 条）
反应条件
1: 4-methyl-benzaldehyde; allyl-trimethyl-silane With lithium boron tetrafluoride in dichloromethane; acetonitrile
T=23°C; 0.5 h;
2: acetic anhydride in dichloromethane; acetonitrile
T=23°C; 2.5 h; Further stages.;
参考文献
Yadav; Reddy, B.V. Subba; Vishnumurthy; Chary, Ch. Janardhana
Tetrahedron Letters, 2007 , vol. 48, # 33 p. 5915 - 5918
反应条件
indium(III) chloride in dichloromethane
T=20°C; 7 h;
参考文献
Yadav; Subba Reddy; Madhuri; Sabitha
Chemistry Letters, 2001 , # 1 p. 18 - 19
反应条件
indium in tetrahydrofuran; water
T=20°C; allylation; 3 h;
参考文献
Yadav; Subba Reddy; Kiran Kumar Reddy
Tetrahedron Letters, 2000 , vol. 41, # 15 p. 2695 - 2697
反应条件
1: 1.) Mg / 1.) ether, 2.) ether, reflux, 20 min
2: 13 percent / pyridine / 36 h / Ambient temperature
View Scheme
参考文献
Hixson; Franke; Gere; Xing
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3601 - 3610
反应条件
in pyridine
36 h; Ambient temperature;
参考文献
Hixson; Franke; Gere; Xing
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3601 - 3610
反应条件
in acetonitrile
8 h; Irradiation;
参考文献
Hixson; Franke; Gere; Xing
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3601 - 3610
反应条件
potassium acetate in acetic anhydride
T=60.4°C; ΔH(excit.), ΔS(excit.), var. temp.; Rate constantThermodynamic data;
参考文献
Wiberg, Kenneth B.; Shobe, David; Nelson, Gordon L.
Journal of the American Chemical Society, 1993 , vol. 115, # 23 p. 10645 - 10652
反应条件
potassium acetate in acetic anhydride
T=110°C; ΔH(excit.), ΔS(excit.), var. temp.; other substituted cis- and trans-cyclobutyl tosylates; Rate constantThermodynamic dataMechanism;
参考文献
Wiberg, Kenneth B.; Shobe, David; Nelson, Gordon L.
Journal of the American Chemical Society, 1993 , vol. 115, # 23 p. 10645 - 10652
反应条件
in acetonitrile
Ambient temperatureIrradiationsinglet lifetimes; Quantum yieldRate constantMechanism;
参考文献
Hixson; Franke; Gere; Xing
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3601 - 3610
反应条件
triethylamine
Multistep reaction;
参考文献
Sakito, Yoji; Suzukamo, Gohfu
Chemistry Letters, 1986 , p. 621 - 624
