苄基氮杂-15-冠醚-5合成路线 （共 13 条）
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal
参考文献
Schultz,R.A.; White,B.D.; Dishong,D.M.
Journal of the American Chemical Society, 1985 , vol. 107, p. 6659
反应条件
tetrabutylammomium bromide; sodium hydroxide in water; benzene
T=70°C; 10 h; Reagent/catalyst;
参考文献
Luk'yanenko; Basok; Kulygina, E. Yu.; Bogashchenko, T. Yu.; Yakovenko
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 10 p. 1345 - 1352
Zh. Org. Khim., 2012 , vol. 48, # 10 p. 1350 - 1357,8
反应条件
sodium carbonate in toluene
3 h; Heating;
参考文献
Katritzky, Alan R.; Denisko, Olga V.; Belyakov, Sergei A.; Schall, Otto F.; Gokel, George W.
Journal of Organic Chemistry, 1996 , vol. 61, # 21 p. 7578 - 7584
反应条件
1: 78 percent / Na2CO3 / acetonitrile / 20 h / 80 °C
2: 46 percent / 50 percent NaH / tetrahydrofuran / 20 h / Heating
View Scheme
参考文献
Schultz,R.A.; White,B.D.; Dishong,D.M.
Journal of the American Chemical Society, 1985 , vol. 107, p. 6659
反应条件
sodium carbonate in acetonitrile
Heating;
参考文献
Sakamoto, Hidefumi; Kimura, Keiichi; Koseki, Yasuaki; Matsuo, Mitsunori; Shono, Toshiyuki
Journal of Organic Chemistry, 1986 , vol. 51, # 25 p. 4974 - 4979
反应条件
1: Na2CO3
2: NaH / tetrahydrofuran
View Scheme
参考文献
Schultz, Rose Ann; Dishong, Dennis M.; Gokel, George W.
Tetrahedron Letters, 1981 , vol. 22, # 28 p. 2623 - 2626
反应条件
1: LiAlH4 / tetrahydrofuran / Heating
2: K2CO3 / acetonitrile
View Scheme
参考文献
Johnson,M.R. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1979 , p. 357 - 371
反应条件
1: (i) NaH, THF, (ii) /BRN= 632509/
2: LiAlH4 / tetrahydrofuran / Heating
3: K2CO3 / acetonitrile
View Scheme
参考文献
Johnson,M.R. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1979 , p. 357 - 371
反应条件
1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / dichloromethane; water / 6.5 h
2: sodium hydroxide; tetrabutylammomium bromide / water; benzene / 10 h / 70 °C
View Scheme
参考文献
Luk'yanenko; Basok; Kulygina, E. Yu.; Bogashchenko, T. Yu.; Yakovenko
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 10 p. 1345 - 1352
Zh. Org. Khim., 2012 , vol. 48, # 10 p. 1350 - 1357,8
反应条件
potassium carbonate in acetonitrile
参考文献
Johnson,M.R. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1979 , p. 357 - 371
