potassium phosphate; 1,3-(4-Ph-OMe)2-5-Ph-1,3,4-triazinium perchlorate in 1,4-dioxane T=80°C; 33 h;

1: diisobutylaluminium hydride / diethyl ether / 0 °C 2: pyridine / dichloromethane / 0 - 20 °C 3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C 4: tris-(dibenzylideneacetone)dipalladium(0); triphenylphosphine / tetrahydrofuran / 24 h / 20 °C / |Schlenk technique; |Inert atmosphere View Scheme

sodium iodide in acetone Heating12-24 h;