N-羟基-3,5-二甲氧基苯甲酰胺合成路线 (共 3 条)
反应条件
N-ethyl-N,N-diisopropylamine; 4-nitrophenylsulfonyl chloride in tetrahydrofuran T=0°C; Lossen Rearrangement; 2 h; Inert atmosphere;
参考文献
Yoganathan, Sabesan; Miller, Scott J.
Organic Letters, 2013 , vol. 15, # 3 p. 602 - 605
反应条件
hydroxylamine in water; acetonitrile
T=23°C; 14 h;
参考文献
Yoganathan, Sabesan; Miller, Scott J.
Organic Letters, 2013 , vol. 15, # 3 p. 602 - 605
反应条件
1: acetonitrile / 1 h / 20 °C
2: hydroxylamine / acetonitrile; water / 14 h / 23 °C
View Scheme
参考文献
Yoganathan, Sabesan; Miller, Scott J.
Organic Letters, 2013 , vol. 15, # 3 p. 602 - 605