1,8-二甲氧基-3-甲基蒽酮合成路线 （共 13 条）
反应条件
hydrogen bromide; acetic acid 0.5 h; Heating;
参考文献
Nicoletti, Teresa M.; Raston, Colin L.; Sargent, Melvyn V.
Journal of the Chemical Society, Chemical Communications, 1988 , p. 1491 - 1493
参考文献
Oesterle
Archiv der Pharmazie (Weinheim, Germany), 1905 , vol. 243, p. 438
反应条件
potassium carbonate in acetone
12 h; Reflux;
参考文献
Grover, Jagdeep; Kumar, Vivek; Singh, Vikram; Bairwa, Khemraj; Sobhia, M. Elizabeth; Jachak, Sanjay M.
European Journal of Medicinal Chemistry, 2014 , vol. 80, p. 47 - 56
反应条件
potassium carbonate in acetone
16 h; Heating;
参考文献
Koyama; Takahashi; Chou; Darzynkiewicz; Kapuscinski; Kelly; Watanabe
Journal of Medicinal Chemistry, 1989 , vol. 32, # 7 p. 1594 - 1599
反应条件
chromium(VI) oxide; acetic acid
0.25 h; Heating;
参考文献
Nicoletti, Teresa M.; Raston, Colin L.; Sargent, Melvyn V.
Journal of the Chemical Society, Chemical Communications, 1988 , p. 1491 - 1493
参考文献
Savard, Jacques; Brassard, Paul
Tetrahedron, 1984 , vol. 40, # 18 p. 3455 - 3464
反应条件
sulfuric acid; oxygen
1.) Et2O, irradiation, 30 deg C, 1.5 h, 2.) acetone, room temperature 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Miyabe, Hideto; Torieda, Mayumi; Inoue, Kyoko; Tajiri, Kazumi; Kiguchi, Toshiko; Naito, Takeaki
Journal of Organic Chemistry, 1998 , vol. 63, # 13 p. 4397 - 4407
反应条件
lithium diisopropyl amide
1.) THF, hexane, -78 deg C, 10 min, 2.) THF, hexane, -40 deg C to RT, 2 h; Yield given. Multistep reaction;
参考文献
Khanapure; Reddy; Biehl
Journal of Organic Chemistry, 1987 , vol. 52, # 26 p. 5685-5690
反应条件
lithium diisopropyl amide
1.) THF, hexane, -78 deg C, 10 min, 2.) THF, hexane, from -40 deg C to RT, 2 h; Yield given. Multistep reaction;
参考文献
Khanapure; Reddy; Biehl
Journal of Organic Chemistry, 1987 , vol. 52, # 26 p. 5685-5690
反应条件
N,N-dimethyl-formamide
参考文献
Koyama, Masao; Kelly, T. Ross; Watanabe, Kyoichi A.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 2 p. 283 - 284
