2,2-二甲基-5-(2-四氢吡咯亚基合成路线 （共 5 条）
反应条件
boric acid T=180°C; 0.75 h;
参考文献
Bacos, Daniel; Celerier, Jean-Pierre; Lhommet, Gerard
Tetrahedron Letters, 1987 , vol. 28, # 21 p. 2353 - 2354
参考文献
Fasseur, Dominique; Rigo, Benoit; Leduc, Catherine; Cauliez, Pascal; Couturier, Daniel
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 5 p. 1285 - 1291
反应条件
RuCl2(tricyclohexylphosphine)2(benzylidene) in benzene
T=120°C; 36 h; Sealed tubeInert atmosphere;
参考文献
Koduri, Naga Durgarao; Scott, Halee; Hileman, Bethany; Cox, Justin D.; Coffin, Michael; Glicksberg, Lindsay; Hussaini, Syed R.
Organic Letters, 2012 , vol. 14, # 2 p. 440 - 443
反应条件
triethylamine in dichloromethane
Eschenmoser Sulfide Contraction; 1 h; Reagent/catalyst;
参考文献
Koduri, Naga Durgarao; Hileman, Bethany; Cox, Justin D.; Scott, Halee; Hoang, Phuong; Robbins, Alexa; Bowers, Kyle; Tsebaot, Lemma; Miao, Kun; Castaneda, Maria; Coffin, Michael; Wei, Guan; Claridge, Tim D. W.; Roberts, Kenneth P.; Hussaini, Syed Raziullah
RSC Advances, 2013 , vol. 3, # 1 p. 181 - 188
反应条件
1: 4-toluenesulfonyl azide; triethylamine / acetonitrile / 6.5 h / 0 - 20 °C
2: RuCl2(tricyclohexylphosphine)2(benzylidene) / benzene / 36 h / 120 °C / Sealed tube; Inert atmosphere
View Scheme
参考文献
Koduri, Naga Durgarao; Scott, Halee; Hileman, Bethany; Cox, Justin D.; Coffin, Michael; Glicksberg, Lindsay; Hussaini, Syed R.
Organic Letters, 2012 , vol. 14, # 2 p. 440 - 443
