甲基β-D-吡喃葡萄糖苷半水合物合成路线 （共 39 条）
反应条件
1: 56 percent / 2,4,6-trimethylpyridine / dimethylformamide; toluene / 0.5 h / -50 °C 2: 99.5 percent / pyridine / acetonitrile / 1 h / 40 - 50 °C 3: 11 percent / 1,1-dichloromethyl methyl ether, ZnCl2 / 4 h / 80 °C 4: 94 percent / thiourea / methanol / 3 h / 50 °C View Scheme
参考文献
Ziegler, Thomas; Kovac, Pavol; Glaudemans, Cornelis P.J.
Carbohydrate Research, 1989 , vol. 194, p. 185 - 198
反应条件
1: 12 percent / sodium hydride / 3 h / 100 °C 2: titanium tetrachloride / CH2Cl2 / 0.08 h / Ambient temperature View Scheme
参考文献
Koto, Shinkiti; Morishima, Naohiko; Kawahara, Reiko; Ishikawa, Katsuhiko; Zen, Shonosuke
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 4 p. 1092 - 1096
反应条件
1: pyridine, N,N'-dimethylaminopyridine / CH2Cl2 / Ambient temperature 2: pyridine 3: 3.5M H2SO4-CrO3 / acetone / 0 °C View Scheme
参考文献
Rej, Rabindra N.; Glushka, John N.; Chew, Warren; Perlin, Arthur S.
Carbohydrate Research, 1989 , vol. 189, p. 135 - 148
反应条件
dinitrogen tetraoxide und Behandeln des Reaktionsprodukts mit Diazomethan in Aether und Behandeln des danach isolierten Reaktionsprodukts mit Acetanhydrid und Pyridin;
参考文献
Hardegger; Spitz
Helvetica Chimica Acta, 1950 , vol. 33, p. 337,341
反应条件
pyridine; dinitrogen tetraoxide Reaktion ueber mehrere Stufen;
参考文献
Hardegger; Spitz
Helvetica Chimica Acta, 1950 , vol. 33, p. 337,341
反应条件
water; oxygen; sodium hydrogencarbonate in Gegenwart von Platin und Erhitzen des Reaktionsprodukts mit wasserhaltiger Ameisensaeure;
参考文献
Barker et al.
Chemistry and Industry (London, United Kingdom), 1951 , p. 970
反应条件
1: 12 percent / sodium hydride / 3 h / 100 °C 2: titanium tetrachloride / CH2Cl2 / 0.08 h / Ambient temperature View Scheme
参考文献
Koto, Shinkiti; Morishima, Naohiko; Kawahara, Reiko; Ishikawa, Katsuhiko; Zen, Shonosuke
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 4 p. 1092 - 1096
反应条件
1: water / acetonitrile / 50 °C / Enzymatic reaction 2: almond meal cross-linked with glutaraldehyde / water / 168 h / 50 °C / Enzymatic reaction View Scheme
参考文献
Wang, Qinqqin; Yu, Huilei; Zhao, Na; Li, Chunxiu; Shang, Yazhuo; Liu, Honglai; Xu, Jianhe
Chinese Journal of Catalysis, 2012 , vol. 33, # 2-3 p. 275 - 280
参考文献
Oldham; Rutherford
Journal of the American Chemical Society, 1932 , vol. 54, p. 366,377
Full Text Show Details
Hess; Stenzel
Chemische Berichte, 1935 , vol. 68, p. 981,988
参考文献
Bragg et al.
Canadian Journal of Chemistry, 1959 , vol. 37, p. 1412,1414
Full Text Show Details
Jones et al.
Canadian Journal of Chemistry, 1960 , vol. 38, p. 1122
Full Text Show Details
Hess; Stenzel
Chemische Berichte, 1935 , vol. 68, p. 981,988
