1-苯基-1H-吡唑-4-甲腈合成路线 （共 15 条）
参考文献
Takamizawa; Hayashi
Yakugaku Zasshi, 1959 , vol. 79, p. 339,343
Chem.Abstr., 1959 , p. 16115
反应条件
hydrogenchloride; acetic acid; sodium nitrite in water
T=20°C; 20 h;
参考文献
Moyano, Elizabeth L.; Colomer, Juan Pablo; Yranzo, Gloria I.
European Journal of Organic Chemistry, 2008 , # 19 p. 3377 - 3381
反应条件
hydrogenchloride; acetic acid; sodium nitrite in water
T=20°C; 20 h;
参考文献
Moyano, Elizabeth L.; Colomer, Juan Pablo; Yranzo, Gloria I.
European Journal of Organic Chemistry, 2008 , # 19 p. 3377 - 3381
反应条件
tert.-butylnitrite in tetrahydrofuran
2 h; Reflux;
参考文献
Dos Santos, Mauricio S.; Bernardino, Alice M. R.; Pinheiro, Luiz C. S.; Canto-Cavalheiro, Marilene M.; Leon, Leonor L.
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 6 p. 1425 - 1428
反应条件
hydrogenchloride; acetic acid; sodium nitrite in water
T=20°C; 6 h; Irradiation;
参考文献
Moyano, Elizabeth L.; Colomer, Juan Pablo; Yranzo, Gloria I.
European Journal of Organic Chemistry, 2008 , # 19 p. 3377 - 3381
反应条件
NH2OH*H2O in formic acid
6 h; Reflux;
参考文献
Dos Santos, Mauricio S.; Gomes, Adriana O.; Bernardino, Alice M. R.; De Souza, Marcos C.; Khan, Misbahul A.; De Brito, Monique A.; Castro, Helena C.; Abreu, Paula A.; Rodrigues, Carlos R.; De Leo, Rosa M. M.; Leon, Leonor L.; Canto-Cavalheirr, Marilene M.
Journal of the Brazilian Chemical Society, 2011 , vol. 22, # 2 p. 352 - 358
反应条件
hydrogenchloride; sodium nitrite in ethanol; water
T=20°C; 20 h;
参考文献
Moyano, Elizabeth L.; Colomer, Juan Pablo; Yranzo, Gloria I.
European Journal of Organic Chemistry, 2008 , # 19 p. 3377 - 3381
反应条件
2-aminopyridine; Cu(NO3)2*3H2O; oxygen; silver carbonate in N,N-dimethyl-formamide
T=150°C; 24 h; Schlenk technique;
参考文献
Pawar, Amit B.; Chang, Sukbok
Chemical Communications, 2014 , vol. 50, # 4 p. 448 - 450
反应条件
acetic acid in ethanol
1 h; Heating;
参考文献
Jachak, Madhukar; Kriessmann, Ulrike; Mittelbach, Martin; Junek, Hans
Monatshefte fuer Chemie, 1993 , vol. 124, p. 199 - 208
反应条件
1: sodium acetate / ethanol / 0.67 h / Reflux
2: tert.-butylnitrite / tetrahydrofuran / 2 h / Reflux
View Scheme
参考文献
Dos Santos, Mauricio S.; Gomes, Adriana O.; Bernardino, Alice M. R.; De Souza, Marcos C.; Khan, Misbahul A.; De Brito, Monique A.; Castro, Helena C.; Abreu, Paula A.; Rodrigues, Carlos R.; De Leo, Rosa M. M.; Leon, Leonor L.; Canto-Cavalheirr, Marilene M.
Journal of the Brazilian Chemical Society, 2011 , vol. 22, # 2 p. 352 - 358
