4,5-亚甲基二硫代-1,3-二硫杂环戊烯-2-硫酮合成路线 （共 12 条）
反应条件
mercury(II) diacetate in tetrahydrofuran; acetic acid 0.5 h; Ambient temperature;
参考文献
Yamada, Jun-Ichi; Satoki, Shyuji; Mishima, Sachinori; Akashi, Nobutaka; Takahashi, Kouhei; Masuda, Nobuyuki; Nishimoto, Yasushi; Takasaki, Satoshi; Anzai, Hiroyuki
Journal of Organic Chemistry, 1996 , vol. 61, # 12 p. 3987 - 3995
反应条件
diiodomethane; sodium methylate in tetrahydrofuran
参考文献
Sony Corporation
Patent: US7425722 B2, 2008 ;
Location in patent: Page/Page column 12-14 ;
反应条件
in tetrahydrofuran
1.5 h; Heating;
参考文献
Yamada, Jun-Ichi; Tanaka, Satoru; Segawa, Junko; Hamasaki, Miho; Hagiya, Kenji; Anzai, Hiroyuki; Nishikawa, Hiroyuki; Ikemoto, Isao; Kikuchi, Koichi
Journal of Organic Chemistry, 1998 , vol. 63, # 12 p. 3952 - 3960
反应条件
sodium methylate
1.) THF, 45 min, 2.) 24 h; Yield given. Multistep reaction;
参考文献
Schulz, Reinhard; Schweig, Armin; Hartke, Klaus; Koester, Joachim
Journal of the American Chemical Society, 1983 , vol. 105, # 14 p. 4519 - 4528
反应条件
in acetone
4 h; Heating;
参考文献
Veldhuizen, Yvonne S. J.; Veldman, Nora; Spek, Anthony L.; Cassoux, Patrick; Carlier, Roger; Mulder, Martijn J. J.; Haasnoot, Jaap G.; Reedijk, Jan
Journal of the Chemical Society - Dalton Transactions, 1998 , # 18 p. 2989 - 2993
反应条件
in acetone
1) 2 h, RT, 2) 4 h, reflux;
参考文献
Poleschner, H.; John, W.; Hoppe, F.; Fanghaenel, E.
Journal fuer Praktische Chemie (Leipzig), 1983 , vol. 325, # 6 p. 957 - 975
反应条件
tetrabutylammomium bromide; zinc dibromide
2.) acetone, RT, 7 d; Yield given. Multistep reaction;
参考文献
Laversanne, R.; Dupart, E.; Delhaes, P.
Molecular Crystals and Liquid Crystals (1969-1991), 1986 , vol. 137, p. 179 - 190
参考文献
Saito, Gunzi; Hayashi, Hitoshi; Enoki, Toshiaki; Inokuchi, Hiroo
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 120, p. 341 - 344
反应条件
triethyl phosphite
T=75 - 80°C; 2 h;
参考文献
Misaki, Yohji; Nishikawa, Hiroyuki; Fujiwara, Hideki; Kawakami, Kazuya; Yamabe, Tokio; et al.
Journal of the Chemical Society, Chemical Communications, 1992 , # 19 p. 1408 - 1409
反应条件
phosphorous acid trimethyl ester in benzene
4 h; Heating;
参考文献
Papavassiliou, G.C.; Zambounis, J.S.; Mousdis, G.A.; Gionis, V.; Yiannopoulos, S.Y.
Molecular Crystals and Liquid Crystals (1969-1991), 1988 , vol. 156, p. 269 - 276
