2-氨基-6-甲基-4(3H)-蝶啶酮合成路线 (共 4 条)
参考文献
Storm et al.
Journal of Organic Chemistry, 1971 , vol. 36, p. 3925
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Karrer; Schwyzer
Helvetica Chimica Acta, 1949 , vol. 32, p. 423,432,
Helvetica Chimica Acta, 1950 , vol. 33, p. 39,43
反应条件
1: 40 percent / 4-dimethylaminopyridine / 3 h / Heating
2: 44 percent / 4-chlorophenyl phosphorodichloridate, pyridine / 48 h / Ambient temperature
3: 96 percent / aq. NH3 / dioxane / 0.5 h / Ambient temperature
4: 89 percent / aq. NH3 / dioxane / 96 h / Ambient temperature
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参考文献
Taylor, Edward C.; Otiv, S. R.; Durucasu, Inci
Heterocycles, 1993 , vol. 36, # 8 p. 1883 - 1895
反应条件
2: ozone / anschliessend Erwaermen mit wss. H2O2 in wss. HCl
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参考文献
Karrer; Feigl
Helvetica Chimica Acta, 1951 , vol. 34, p. 2155,2156
参考文献
Mowat et al.
Journal of the American Chemical Society, 1948 , vol. 79, p. 14,18