1,5-二氢吡咯并[2,3-f]吲哚合成路线 （共 10 条）
反应条件
potassium hydroxide in methanol
参考文献
Prasad; Burchat; Weeratunga; Watts; Dmitrienko
Tetrahedron Letters, 1991 , vol. 32, # 38 p. 5035 - 5038
反应条件
(bis(N-methylimidazol-2-yl)methane)dicarbonylrhodium(I) tetraphenylborate in THF-d8 (tetrahydrofuran-d8)
T=60°C; 7.2 h;
参考文献
Clentsmith, Guy K.B.; Field, Leslie D.; Messerle, Barbara A.; Shasha, Adelle; Turner, Peter
Tetrahedron Letters, 2009 , vol. 50, # 13 p. 1469 - 1471
反应条件
1: p-TSA
2: 1) HNO3, H2SO4, 2) H2 / 2) Pt / 2) EtOH
3: 1) Na2CO3, 2) NEt3 / 1) EtOH, 2) hexane
4: 86 percent / TFA, (CF3CO)2O
5: 76 percent / DDQ / benzene / Heating
6: 91 percent / KOH / methanol
View Scheme
参考文献
Prasad; Burchat; Weeratunga; Watts; Dmitrienko
Tetrahedron Letters, 1991 , vol. 32, # 38 p. 5035 - 5038
反应条件
1: 1) HNO3, H2SO4, 2) H2 / 2) Pt / 2) EtOH
2: 1) Na2CO3, 2) NEt3 / 1) EtOH, 2) hexane
3: 86 percent / TFA, (CF3CO)2O
4: 76 percent / DDQ / benzene / Heating
5: 91 percent / KOH / methanol
View Scheme
参考文献
Prasad; Burchat; Weeratunga; Watts; Dmitrienko
Tetrahedron Letters, 1991 , vol. 32, # 38 p. 5035 - 5038
反应条件
1: NaHSO3, KOH / H2O / 1 h / Heating
2: 8 percent / Pd/C / 0.08 h / Heating
View Scheme
参考文献
Samsoniya, Sh. A.; Kadzhrishvili, D. O.; Gordeev, E. N.; Zhigachev, V. E.; Kurkovskaya, L. N.; Suvorov, N. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 4 p. 382 - 385
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 4 p. 504 - 507
反应条件
1: NaHSO3, KOH / H2O / 1 h / Heating
2: 8 percent / Pd/C / 0.08 h / Heating
View Scheme
参考文献
Samsoniya, Sh. A.; Kadzhrishvili, D. O.; Gordeev, E. N.; Zhigachev, V. E.; Kurkovskaya, L. N.; Suvorov, N. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 4 p. 382 - 385
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 4 p. 504 - 507
反应条件
1: 78 percent / dimethylformamide / 90 - 120 °C
2: 50 percent / H2 / 10percent Pd-C / ethyl acetate / 760 Torr / Ambient temperature
View Scheme
参考文献
Berlin, A.; Bradamante, S.; Ferraccioli, R.; Pagani, G. A.; Sannicolo, F.
Journal of the Chemical Society, Chemical Communications, 1987 , # 15 p. 1176 - 1177
反应条件
1: 1) Na2CO3, 2) NEt3 / 1) EtOH, 2) hexane
2: 86 percent / TFA, (CF3CO)2O
3: 76 percent / DDQ / benzene / Heating
4: 91 percent / KOH / methanol
View Scheme
参考文献
Prasad; Burchat; Weeratunga; Watts; Dmitrienko
Tetrahedron Letters, 1991 , vol. 32, # 38 p. 5035 - 5038
反应条件
1: 86 percent / TFA, (CF3CO)2O
2: 76 percent / DDQ / benzene / Heating
3: 91 percent / KOH / methanol
View Scheme
参考文献
Prasad; Burchat; Weeratunga; Watts; Dmitrienko
Tetrahedron Letters, 1991 , vol. 32, # 38 p. 5035 - 5038
反应条件
palladium on activated charcoal
0.0833333 h; Heating;
参考文献
Samsoniya, Sh. A.; Kadzhrishvili, D. O.; Gordeev, E. N.; Zhigachev, V. E.; Kurkovskaya, L. N.; Suvorov, N. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 4 p. 382 - 385
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 4 p. 504 - 507
